3,4-bis(hexyloxy)-2-{4-[N,N-bis[2-(acetyloxy)ethyl]amino]styryl}thiophene-5-carboxaldehyde

Base Information

Chemical Name:3,4-bis(hexyloxy)-2-{4-[N,N-bis[2-(acetyloxy)ethyl]amino]styryl}thiophene-5-carboxaldehyde
CAS No.:1248703-67-4
Molecular Formula:C₃₃H₄₇NO₇S
Molecular Weight:601.805
Hs Code.:

Synonyms:3,4-bis(hexyloxy)-2-{4-[N,N-bis[2-(acetyloxy)ethyl]amino]styryl}thiophene-5-carboxaldehyde

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Chemical Property of 3,4-bis(hexyloxy)-2-{4-[N,N-bis[2-(acetyloxy)ethyl]amino]styryl}thiophene-5-carboxaldehyde

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Technology Process of 3,4-bis(hexyloxy)-2-{4-[N,N-bis[2-(acetyloxy)ethyl]amino]styryl}thiophene-5-carboxaldehyde

There total 5 articles about 3,4-bis(hexyloxy)-2-{4-[N,N-bis[2-(acetyloxy)ethyl]amino]styryl}thiophene-5-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 1248703-62-9
3,4-bis(hexyloxy)-2-{4-[N,N-di[2-(acetyloxy)ethyl]amino]styryl}thiophene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1248703-67-4
3,4-bis(hexyloxy)-2-{4-[N,N-bis[2-(acetyloxy)ethyl]amino]styryl}thiophene-5-carboxaldehyde

Guidance literature:: With trichlorophosphate; at 0 - 90 ℃;
DOI:10.1002/poc.1772

Reference yield:

: 1248703-57-2
3,4-bis(hexyloxy)thiophen-2-methanol

: 1248703-67-4
3,4-bis(hexyloxy)-2-{4-[N,N-bis[2-(acetyloxy)ethyl]amino]styryl}thiophene-5-carboxaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: chloroform / 3 h / Reflux

2: sodium hydride / diethyl ether / 24 h / 20 °C / Inert atmosphere

3: trichlorophosphate / 0 - 90 °C

With sodium hydride; trichlorophosphate; In diethyl ether; chloroform; 2: Wittig reaction / 3: Vilsmeier formylation;
DOI:10.1002/poc.1772

Reference yield:

: 1248703-59-4
Br^(1-)*C₃₅H₄₄O₂PS⁽¹⁺⁾

: 1248703-67-4
3,4-bis(hexyloxy)-2-{4-[N,N-bis[2-(acetyloxy)ethyl]amino]styryl}thiophene-5-carboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / diethyl ether / 24 h / 20 °C / Inert atmosphere

2: trichlorophosphate / 0 - 90 °C

With sodium hydride; trichlorophosphate; In diethyl ether; 1: Wittig reaction / 2: Vilsmeier formylation;
DOI:10.1002/poc.1772