1H,1'H-1,1'-hexanedioyl-bis-imidazole

Base Information

• Chemical Name: 1H,1'H-1,1'-hexanedioyl-bis-imidazole
• CAS No.: 7288-34-8
• Molecular Formula: C₁₂H₁₄N₄O₂
• Molecular Weight: 246.269
• Mol file: 7288-34-8.mol

Synonyms:1H,1'H-1,1'-hexanedioyl-bis-imidazole

Chemical Property of 1H,1'H-1,1'-hexanedioyl-bis-imidazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1H,1'H-1,1'-hexanedioyl-bis-imidazole

There total 3 articles about 1H,1'H-1,1'-hexanedioyl-bis-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Adipic acid (124-04-9) + 1,1'-carbonyldiimidazole (530-62-1) → 1H,1'H-1,1'-hexanedioyl-bis-imidazole (7288-34-8)

Guidance literature:

In N,N-dimethyl acetamide; at 40 ℃;

DOI:10.1021/ja00198a068

Reference yield:

1H-imidazole (288-32-4) + Adipic acid dichloride (111-50-2) → 1H,1'H-1,1'-hexanedioyl-bis-imidazole (7288-34-8)

Guidance literature:

With tetrahydrofuran;

Reference yield:

→ 1H,1'H-1,1'-hexanedioyl-bis-imidazole (7288-34-8)

Guidance literature:

Adipinsaeure, N,N'-Thionyl-diimidazol (nach Staab, Wendel, Ang. Ch. 73 (1961) 26);

upstream raw materials:

1H-imidazole

Adipic acid dichloride

Adipic acid

1,1'-carbonyldiimidazole

Downstream raw materials:

N,N'-diphenyladipamide