2'-azido-5-deoxy-2,3-O-ethylene-1-O-mesitylenesuphonyl-α-L-sorbopyranose

Base Information

Chemical Name:2'-azido-5-deoxy-2,3-O-ethylene-1-O-mesitylenesuphonyl-α-L-sorbopyranose
CAS No.:99042-73-6
Molecular Formula:C₁₇H₂₃N₃O₇S
Molecular Weight:413.452
Hs Code.:

Synonyms:2'-azido-5-deoxy-2,3-O-ethylene-1-O-mesitylenesuphonyl-α-L-sorbopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-azido-5-deoxy-2,3-O-ethylene-1-O-mesitylenesuphonyl-α-L-sorbopyranose

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Technology Process of 2'-azido-5-deoxy-2,3-O-ethylene-1-O-mesitylenesuphonyl-α-L-sorbopyranose

There total 3 articles about 2'-azido-5-deoxy-2,3-O-ethylene-1-O-mesitylenesuphonyl-α-L-sorbopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 99042-68-9
4,5-anhydro-2,3-O-ethylene-1-O-mesitylenesulphonyl-β-D-fructopyranose

: 99042-73-6
2'-azido-5-deoxy-2,3-O-ethylene-1-O-mesitylenesuphonyl-α-L-sorbopyranose

Guidance literature:: With sodium azide; ammonium chloride; In ethanol; water; for 16h; Heating;

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 99042-73-6
2'-azido-5-deoxy-2,3-O-ethylene-1-O-mesitylenesuphonyl-α-L-sorbopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / pyridine / 96 h / Ambient temperature

2: 76 percent / 1M sodium methoxide / methanol / 3 h / Heating

3: 91 percent / sodium azide, ammonium chloride / ethanol; H₂O / 16 h / Heating

With pyridine; sodium azide; ammonium chloride; sodium methylate; In methanol; ethanol; water;

Reference yield:

: 99042-60-1
2'-chloroethyl 1,4-di-O-mesitylenesulphonyl-β-D-fructopyranoside

: 99042-73-6
2'-azido-5-deoxy-2,3-O-ethylene-1-O-mesitylenesuphonyl-α-L-sorbopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / 1M sodium methoxide / methanol / 3 h / Heating

2: 91 percent / sodium azide, ammonium chloride / ethanol; H₂O / 16 h / Heating

With sodium azide; ammonium chloride; sodium methylate; In methanol; ethanol; water;