methyl (R,R)-2-chloro-3-phenyl-3-(p-toluenesulfonylamino)propanimidate hydrochloride

Base Information

Chemical Name:methyl (R,R)-2-chloro-3-phenyl-3-(p-toluenesulfonylamino)propanimidate hydrochloride
CAS No.:1275616-34-6
Molecular Formula:C₁₇H₁₉ClN₂O₃S*ClH
Molecular Weight:403.329
Hs Code.:

Synonyms:methyl (R,R)-2-chloro-3-phenyl-3-(p-toluenesulfonylamino)propanimidate hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (R,R)-2-chloro-3-phenyl-3-(p-toluenesulfonylamino)propanimidate hydrochloride

Chemical Property:

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Technology Process of methyl (R,R)-2-chloro-3-phenyl-3-(p-toluenesulfonylamino)propanimidate hydrochloride

There total 2 articles about methyl (R,R)-2-chloro-3-phenyl-3-(p-toluenesulfonylamino)propanimidate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: methyl (R(S),R,R)-2-chloro-3-phenyl-3-(p-toluenesulfonylamino)-N-tert-butanesulfinylpropanimidate

: 1275616-34-6
methyl (R,R)-2-chloro-3-phenyl-3-(p-toluenesulfonylamino)propanimidate hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; diethyl ether; at 20 ℃; for 1h;
DOI:10.1021/jo200082w

Reference yield:

: 51608-60-7
N-(benzylidene)-p-methylbenzenesulfonamide

: 1275616-34-6
methyl (R,R)-2-chloro-3-phenyl-3-(p-toluenesulfonylamino)propanimidate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C

1.2: 0.5 h / -78 °C

2.1: hydrogenchloride / 1,4-dioxane; diethyl ether / 1 h / 20 °C

With hydrogenchloride; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; diethyl ether; 1.2: Mannich type reaction;
DOI:10.1021/jo200082w