4-<4-(1-Phenyl-5-methylpyrazolyl)>-2-thiazolylacetic acid

Base Information

Chemical Name:4-<4-(1-Phenyl-5-methylpyrazolyl)>-2-thiazolylacetic acid
CAS No.:137577-02-7
Molecular Formula:C₁₅H₁₃N₃O₂S
Molecular Weight:299.353
Hs Code.:

Synonyms:4-<4-(1-Phenyl-5-methylpyrazolyl)>-2-thiazolylacetic acid

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Chemical Property of 4-<4-(1-Phenyl-5-methylpyrazolyl)>-2-thiazolylacetic acid

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Technology Process of 4-<4-(1-Phenyl-5-methylpyrazolyl)>-2-thiazolylacetic acid

There total 3 articles about 4-<4-(1-Phenyl-5-methylpyrazolyl)>-2-thiazolylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 137813-15-1
Methyl 4-<4-(1-phenyl-5-methylpyrazolyl)>-2-thiazolylacetate hydrobromide

: 137577-02-7
4-<4-(1-Phenyl-5-methylpyrazolyl)>-2-thiazolylacetic acid

Guidance literature:: With sodium hydroxide; at 70 ℃; for 0.166667h;
DOI:10.1002/jhet.5570280625

Reference yield:

: 6123-63-3
4-acetyl-5-methyl-1-phenylpyrazole

: 137577-02-7
4-<4-(1-Phenyl-5-methylpyrazolyl)>-2-thiazolylacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / bromine, 48 percent HBr, glacial acetic acid / CHCl₃ / 0.25 h / Ambient temperature

2: 69 percent / acetone / 3 h / Heating

3: 77 percent / 2 N aq. sodium hydroxide / 0.17 h / 70 °C

With sodium hydroxide; hydrogen bromide; bromine; acetic acid; In chloroform; acetone;
DOI:10.1002/jhet.5570280625

Reference yield:

: 137577-00-5
2-bromo-1-(5-methyl-1-phenyl-1H-pyrazol-4-yl)ethan-1-one

: 137577-02-7
4-<4-(1-Phenyl-5-methylpyrazolyl)>-2-thiazolylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / acetone / 3 h / Heating

2: 77 percent / 2 N aq. sodium hydroxide / 0.17 h / 70 °C

With sodium hydroxide; In acetone;
DOI:10.1002/jhet.5570280625