N-(benzylsulfonyl)-4-{[[(4-chlorophenyl)sulfonyl](pyridin-2-ylmethyl)amino]methyl}benzamide

Base Information

Chemical Name:N-(benzylsulfonyl)-4-{[[(4-chlorophenyl)sulfonyl](pyridin-2-ylmethyl)amino]methyl}benzamide
CAS No.:1191066-15-5
Molecular Formula:C₂₇H₂₄ClN₃O₅S₂
Molecular Weight:570.09
Hs Code.:

Synonyms:N-(benzylsulfonyl)-4-{[[(4-chlorophenyl)sulfonyl](pyridin-2-ylmethyl)amino]methyl}benzamide

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Chemical Property of N-(benzylsulfonyl)-4-{[[(4-chlorophenyl)sulfonyl](pyridin-2-ylmethyl)amino]methyl}benzamide

Chemical Property:

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Technology Process of N-(benzylsulfonyl)-4-{[[(4-chlorophenyl)sulfonyl](pyridin-2-ylmethyl)amino]methyl}benzamide

There total 4 articles about N-(benzylsulfonyl)-4-{[[(4-chlorophenyl)sulfonyl](pyridin-2-ylmethyl)amino]methyl}benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 111195-91-6
4-chloro-N-(pyridin-2-ylmethyl)benzenesulfonamide

: 4563-33-1
phenyl-methanesulfonic acid amide

: 1191066-15-5
N-(benzylsulfonyl)-4-{[[(4-chlorophenyl)sulfonyl](pyridin-2-ylmethyl)amino]methyl}benzamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 4h;

Reference yield: 31.0%

: 1191069-57-4
4-{[[(4-chlorophenyl)sulfonyl](pyridin-2-ylmethyl)amino]methyl}benzoic acid

: 4563-33-1
phenyl-methanesulfonic acid amide

: 1191066-15-5
N-(benzylsulfonyl)-4-{[[(4-chlorophenyl)sulfonyl](pyridin-2-ylmethyl)amino]methyl}benzamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 4h;
DOI:10.1016/j.bmcl.2010.04.113

Reference yield:

: 3731-51-9
2-(Aminomethyl)pyridine

: 1191066-15-5
N-(benzylsulfonyl)-4-{[[(4-chlorophenyl)sulfonyl](pyridin-2-ylmethyl)amino]methyl}benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane;