C₉₄H₁₂₂Si₄

Base Information

Chemical Name:C₉₄H₁₂₂Si₄
CAS No.:865096-70-4
Molecular Formula:C₉₄H₁₂₂Si₄
Molecular Weight:1364.34
Hs Code.:

C<sub>94</sub>H<sub>122</sub>Si<sub>4</sub>

Synonyms:C₉₄H₁₂₂Si₄

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Chemical Property of C₉₄H₁₂₂Si₄

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Technology Process of C₉₄H₁₂₂Si₄

There total 17 articles about C₉₄H₁₂₂Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 865096-83-9
C₈₇H₁₁₃ISi₃

: 4526-06-1
trimethylsilyl-1,3-butadiyne

: 865096-70-4
C₉₄H₁₂₂Si₄

Guidance literature:: With copper(l) iodide; diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 35 ℃; for 2h;
DOI:10.1021/jo050926v

Reference yield:

: 1-[(2-bromo-4,5-diiodo)phenyl]-3,3-dimethyltriazene

: 865096-70-4
C₉₄H₁₂₂Si₄

Guidance literature:: Multi-step reaction with 4 steps

1: 4.16 g / CuI; (i-Pr)2NH / Pd(PPh₃)4 / tetrahydrofuran; methanol / 9 h / 50 °C

2: 77 percent / (i-Pr)2NH; CuI / Pd(PPh₃)4 / tetrahydrofuran / 16 h / 80 °C

3: 82 percent / aq. HI / CCl₄; acetonitrile / 0.75 h / 60 °C

4: 73 percent / (i-Pr)2NH; CuI / Pd(PPh₃)4 / tetrahydrofuran / 2 h / 35 °C

With copper(l) iodide; hydrogen iodide; diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; tetrachloromethane; acetonitrile; 1: Sonogashira reaction / 2: Sonogashira reaction / 4: Sonogashira reaction;
DOI:10.1021/jo050926v

Reference yield:

: 865096-73-7
4-amino-3',5'-di-tert-butylbiphenyl

: 865096-70-4
C₉₄H₁₂₂Si₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: 88 percent / BnEt₃NICl₂ / CH₂Cl₂; methanol / 16 h / 20 °C

2.1: aq. HCl; NaNO₂ / acetonitrile; tetrahydrofuran; H₂O / 0.25 h / -5 °C

2.2: 89 percent / K₂CO₃ / acetonitrile; tetrahydrofuran; H₂O / -5 - 20 °C

3.1: 99 percent / (i-Pr)2NH; CuI / Pd(PPh₃)4 / tetrahydrofuran / 8 h / 40 °C

4.1: 99 percent / MeI / 12 h / 140 °C

5.1: 83 percent / (i-Pr)2NH; CuI / Pd(PPh₃)4 / tetrahydrofuran / 12 h / 40 °C

6.1: K₂CO₃ / tetrahydrofuran; methanol / 6 h / 20 °C

7.1: 4.16 g / CuI; (i-Pr)2NH / Pd(PPh₃)4 / tetrahydrofuran; methanol / 9 h / 50 °C

8.1: 77 percent / (i-Pr)2NH; CuI / Pd(PPh₃)4 / tetrahydrofuran / 16 h / 80 °C

9.1: 82 percent / aq. HI / CCl₄; acetonitrile / 0.75 h / 60 °C

10.1: 73 percent / (i-Pr)2NH; CuI / Pd(PPh₃)4 / tetrahydrofuran / 2 h / 35 °C

With hydrogenchloride; copper(l) iodide; hydrogen iodide; potassium carbonate; diisopropylamine; benzyl triethylammonium dichloroiodate; sodium nitrite; methyl iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; water; acetonitrile; 3.1: Sonogashira reaction / 5.1: Sonogashira reaction / 7.1: Sonogashira reaction / 8.1: Sonogashira reaction / 10.1: Sonogashira reaction;
DOI:10.1021/jo050926v