8-hydrazino-7-[2-hydroxy-3-(4-tert-butyl)phenoxyprop-1-yl]-3-methylxanthine

Base Information

Chemical Name:8-hydrazino-7-[2-hydroxy-3-(4-tert-butyl)phenoxyprop-1-yl]-3-methylxanthine
CAS No.:1620289-12-4
Molecular Formula:C₁₉H₂₆N₆O₄
Molecular Weight:402.453
Hs Code.:

Synonyms:8-hydrazino-7-[2-hydroxy-3-(4-tert-butyl)phenoxyprop-1-yl]-3-methylxanthine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-hydrazino-7-[2-hydroxy-3-(4-tert-butyl)phenoxyprop-1-yl]-3-methylxanthine

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Technology Process of 8-hydrazino-7-[2-hydroxy-3-(4-tert-butyl)phenoxyprop-1-yl]-3-methylxanthine

There total 3 articles about 8-hydrazino-7-[2-hydroxy-3-(4-tert-butyl)phenoxyprop-1-yl]-3-methylxanthine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

: 1620289-11-3
8-bromo-7-[2-hydroxy-3-(4-tert-butyl)phenoxyprop-1-yl]-3-methylxanthine

: 1620289-12-4
8-hydrazino-7-[2-hydroxy-3-(4-tert-butyl)phenoxyprop-1-yl]-3-methylxanthine

Guidance literature:: With hydrazine hydrate; In 1,4-dioxane; water; for 0.583333h; Heating;
DOI:10.1007/s10600-014-0998-5

Reference yield:

: 93703-24-3
3-methyl-8-bromoxanthine

: 1620289-12-4
8-hydrazino-7-[2-hydroxy-3-(4-tert-butyl)phenoxyprop-1-yl]-3-methylxanthine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / propan-1-ol / 3 h / Reflux

2: hydrazine hydrate / water; 1,4-dioxane / 0.58 h / Heating

With hydrazine hydrate; triethylamine; In 1,4-dioxane; propan-1-ol; water;
DOI:10.1007/s10600-014-0998-5

Reference yield:

: 3101-60-8
4-tert-butylphenyl 2,3-epoxypropyl ether

: 1620289-12-4
8-hydrazino-7-[2-hydroxy-3-(4-tert-butyl)phenoxyprop-1-yl]-3-methylxanthine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / propan-1-ol / 3 h / Reflux

2: hydrazine hydrate / water; 1,4-dioxane / 0.58 h / Heating

With hydrazine hydrate; triethylamine; In 1,4-dioxane; propan-1-ol; water;
DOI:10.1007/s10600-014-0998-5