1-(4-aminophenyl)-3,5-dihydro-7,8-ethylenedioxy-4H-2,3-benzodiazepin-4-one

Base Information

Chemical Name:1-(4-aminophenyl)-3,5-dihydro-7,8-ethylenedioxy-4H-2,3-benzodiazepin-4-one
CAS No.:874111-16-7
Molecular Formula:C₁₇H₁₅N₃O₃
Molecular Weight:309.324
Hs Code.:

Synonyms:1-(4-aminophenyl)-3,5-dihydro-7,8-ethylenedioxy-4H-2,3-benzodiazepin-4-one

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Chemical Property of 1-(4-aminophenyl)-3,5-dihydro-7,8-ethylenedioxy-4H-2,3-benzodiazepin-4-one

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Technology Process of 1-(4-aminophenyl)-3,5-dihydro-7,8-ethylenedioxy-4H-2,3-benzodiazepin-4-one

There total 3 articles about 1-(4-aminophenyl)-3,5-dihydro-7,8-ethylenedioxy-4H-2,3-benzodiazepin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874111-06-5
[7-(4-nitro-benzoyl)-2,3-dihydro-benzo[1,4]dioxin-6-yl]-acetic acid methyl ester

: 874111-16-7
1-(4-aminophenyl)-3,5-dihydro-7,8-ethylenedioxy-4H-2,3-benzodiazepin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / NH₂NH₂*H₂O / butan-1-ol / 20 h / Heating

2: 92 percent / HCO₂NH₄ / Ni-Raney / ethanol / 2 h / Heating

With ammonium formate; hydrazine hydrate; Ni-Raney; In ethanol; butan-1-ol;
DOI:10.1016/j.bmcl.2005.09.029

Reference yield:

: 25379-88-8
2-(3,4-dihydroxyphenyl)acetic acid methyl ester

: 874111-16-7
1-(4-aminophenyl)-3,5-dihydro-7,8-ethylenedioxy-4H-2,3-benzodiazepin-4-one

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / K₂CO₃ / acetone / 42 h / Heating

2: 54 percent / P₂O₅ / 1,2-dichloro-ethane / 16 h / 20 °C

3: 64 percent / NH₂NH₂*H₂O / butan-1-ol / 20 h / Heating

4: 92 percent / HCO₂NH₄ / Ni-Raney / ethanol / 2 h / Heating

With ammonium formate; phosphorus pentoxide; potassium carbonate; hydrazine hydrate; Ni-Raney; In ethanol; 1,2-dichloro-ethane; acetone; butan-1-ol;
DOI:10.1016/j.bmcl.2005.09.029

Reference yield:

: 25379-89-9
methyl 2-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)acetate

: 874111-16-7
1-(4-aminophenyl)-3,5-dihydro-7,8-ethylenedioxy-4H-2,3-benzodiazepin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / P₂O₅ / 1,2-dichloro-ethane / 16 h / 20 °C

2: 64 percent / NH₂NH₂*H₂O / butan-1-ol / 20 h / Heating

3: 92 percent / HCO₂NH₄ / Ni-Raney / ethanol / 2 h / Heating

With ammonium formate; phosphorus pentoxide; hydrazine hydrate; Ni-Raney; In ethanol; 1,2-dichloro-ethane; butan-1-ol;
DOI:10.1016/j.bmcl.2005.09.029