C₁₂H₁₂I₂O₆

Base Information

Chemical Name:C₁₂H₁₂I₂O₆
CAS No.:1243250-84-1
Molecular Formula:C₁₂H₁₂I₂O₆
Molecular Weight:506.033
Hs Code.:

C<sub>12</sub>H<sub>12</sub>I<sub>2</sub>O<sub>6</sub>

Synonyms:C₁₂H₁₂I₂O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₂I₂O₆

Chemical Property:

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Technology Process of C₁₂H₁₂I₂O₆

There total 1 articles about C₁₂H₁₂I₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 96-32-2
bromoacetic acid methyl ester

: 13064-64-7
2,5-diiodo-1,4-hydroquinone

: 1243250-84-1
C₁₂H₁₂I₂O₆

Guidance literature:: 2,5-diiodo-1,4-hydroquinone; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

bromoacetic acid methyl ester; In N,N-dimethyl-formamide; at 40 ℃; Inert atmosphere;
DOI:10.1021/ma101816z

Reference yield: 48.0%

: 1243250-84-1
C₁₂H₁₂I₂O₆

: 1066-54-2
trimethylsilylacetylene

: 1243250-86-3
C₂₂H₃₀O₆Si₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In ethyl acetate; at 40 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/ma101816z

Reference yield:

: 1243250-84-1
C₁₂H₁₂I₂O₆

: 1243250-87-4
C₁₆H₁₄O₆

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / ethyl acetate / 0.25 h / 40 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere; Darkness

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; ethyl acetate; 1: Sonogashira coupling;
DOI:10.1021/ma101816z