3-(trityl-amino)-N-{6-[3-(trityl-amino)-propionylamino]-9H-fluoren-3-yl}-propionamide

Base Information

• Chemical Name: 3-(trityl-amino)-N-{6-[3-(trityl-amino)-propionylamino]-9H-fluoren-3-yl}-propionamide
• CAS No.: 812653-27-3
• Molecular Formula: C₅₇H₅₀N₄O₂
• Molecular Weight: 823.05

Synonyms:3-(trityl-amino)-N-{6-[3-(trityl-amino)-propionylamino]-9H-fluoren-3-yl}-propionamide

Chemical Property of 3-(trityl-amino)-N-{6-[3-(trityl-amino)-propionylamino]-9H-fluoren-3-yl}-propionamide

Chemical Property:

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Technology Process of 3-(trityl-amino)-N-{6-[3-(trityl-amino)-propionylamino]-9H-fluoren-3-yl}-propionamide

There total 1 articles about 3-(trityl-amino)-N-{6-[3-(trityl-amino)-propionylamino]-9H-fluoren-3-yl}-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2,7-diaminofluorene (55216-61-0) + Trt-βAla-OSu (58995-27-0) → 3-(trityl-amino)-N-{6-[3-(trityl-amino)-propionylamino]-9H-fluoren-3-yl}-propionamide (812653-27-3)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 60 ℃; for 20h;

DOI:10.1016/j.tetlet.2004.10.012

Reference yield: 57.0%

3-(trityl-amino)-N-{6-[3-(trityl-amino)-propionylamino]-9H-fluoren-3-yl}-propionamide (812653-27-3) → N,N'-bis-[3-(trityl-amino)-propyl]-9H-fluorene-3,6-diamine (812653-37-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 72h; Heating;

DOI:10.1016/j.tetlet.2004.10.012

Reference yield:

3-(trityl-amino)-N-{6-[3-(trityl-amino)-propionylamino]-9H-fluoren-3-yl}-propionamide (812653-27-3) → C79H90N8O8

Guidance literature:

Multi-step reaction with 2 steps

1: 57 percent / LiAlH₄ / tetrahydrofuran / 72 h / Heating

2: 85 percent / Et₃N; Mukaiyama's reagent / CH₂Cl₂ / 0.75 h / 25 °C

With lithium aluminium tetrahydride; N-methyl-2-methylpyridinium iodide; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.tetlet.2004.10.012

upstream raw materials:

2,7-diaminofluorene

Trt-βAla-OSu

Downstream raw materials:

N,N'-bis-[3-(trityl-amino)-propyl]-9H-fluorene-3,6-diamine

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