Dodecyl-phosphonic acid mono-((1S,2R,3S,4S,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-fluoro-cyclohexyl) ester

Base Information

Chemical Name:Dodecyl-phosphonic acid mono-((1S,2R,3S,4S,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-fluoro-cyclohexyl) ester
CAS No.:172722-85-9
Molecular Formula:C₄₆H₆₀FO₇P
Molecular Weight:774.95
Hs Code.:

Synonyms:Dodecyl-phosphonic acid mono-((1S,2R,3S,4S,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-fluoro-cyclohexyl) ester

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Chemical Property of Dodecyl-phosphonic acid mono-((1S,2R,3S,4S,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-fluoro-cyclohexyl) ester

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Technology Process of Dodecyl-phosphonic acid mono-((1S,2R,3S,4S,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-fluoro-cyclohexyl) ester

There total 6 articles about Dodecyl-phosphonic acid mono-((1S,2R,3S,4S,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-fluoro-cyclohexyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 3586-98-9
n-dodecylphosphonic acid dichloride

: 172722-84-8
1,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-myo-inositol

: 172722-85-9
Dodecyl-phosphonic acid mono-((1S,2R,3S,4S,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-fluoro-cyclohexyl) ester

Guidance literature:: With base; Ambient temperature;
DOI:10.1016/0040-4039(95)01579-5

Reference yield:

: 172722-79-1
1-O-benzoyl-3,4,5,6-tetra-O-benzyl-myo-inositol

: 172722-85-9
Dodecyl-phosphonic acid mono-((1S,2R,3S,4S,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-fluoro-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / Ac₂O / dimethylsulfoxide

2: NaBH₄, CaCl₂ / methanol / 1 h / 0 °C

3: 32 percent / DAST / CH₂Cl₂ / 0 °C

4: NaOH / H₂O / Ambient temperature

5: 83 percent / base / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; acetic anhydride; 4,4'-diaminostilbene-2,2'-disulfonic acid; calcium chloride; In methanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/0040-4039(95)01579-5

Reference yield:

: 24558-77-8
3,4,5,6-tetra-O-benzyl inositol

: 172722-85-9
Dodecyl-phosphonic acid mono-((1S,2R,3S,4S,5R,6R)-2,3,4,5-tetrakis-benzyloxy-6-fluoro-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / base

2: 88 percent / Ac₂O / dimethylsulfoxide

3: NaBH₄, CaCl₂ / methanol / 1 h / 0 °C

4: 32 percent / DAST / CH₂Cl₂ / 0 °C

5: NaOH / H₂O / Ambient temperature

6: 83 percent / base / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; acetic anhydride; 4,4'-diaminostilbene-2,2'-disulfonic acid; calcium chloride; In methanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/0040-4039(95)01579-5