13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazapentacyclo[22.2.1.1(11,14).0(2,6).0(15,19)]octacosa-1⁽²⁷⁾,9,11,14⁽²⁸⁾,22,24-hexaene

Base Information

• Chemical Name: 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazapentacyclo[22.2.1.1(11,14).0(2,6).0(15,19)]octacosa-1⁽²⁷⁾,9,11,14⁽²⁸⁾,22,24-hexaene
• CAS No.: 244217-88-7
• Molecular Formula: C₃₂H₃₈N₁₀
• Molecular Weight: 562.721

Synonyms:13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazapentacyclo[22.2.1.1(11,14).0(2,6).0(15,19)]octacosa-1⁽²⁷⁾,9,11,14⁽²⁸⁾,22,24-hexaene

Chemical Property of 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazapentacyclo[22.2.1.1(11,14).0(2,6).0(15,19)]octacosa-1⁽²⁷⁾,9,11,14⁽²⁸⁾,22,24-hexaene

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Technology Process of 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazapentacyclo[22.2.1.1(11,14).0(2,6).0(15,19)]octacosa-1⁽²⁷⁾,9,11,14⁽²⁸⁾,22,24-hexaene

There total 1 articles about 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazapentacyclo[22.2.1.1(11,14).0(2,6).0(15,19)]octacosa-1⁽²⁷⁾,9,11,14⁽²⁸⁾,22,24-hexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

3-azapentane-1,5-diamine (111-40-0,98824-35-2) + 1-benzyl-3,5-pyrazoledicarbaldehyde (244217-84-3) → 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazapentacyclo[22.2.1.1(11,14).0(2,6).0(15,19)]octacosa-1(27),9,11,14(28),22,24-hexaene (244217-88-7)

Guidance literature:

In acetonitrile; at 25 ℃;

DOI:10.1021/jm2017144

Reference yield: 83.0%

13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazapentacyclo[22.2.1.1(11,14).0(2,6).0(15,19)]octacosa-1(27),9,11,14(28),22,24-hexaene (244217-88-7) → 13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazatricyclo-[22.2.1.111,14]-octacosa-1(27),11,14(28),24-tetraene (244217-92-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 25 ℃; for 2h;

DOI:10.1021/jm2017144

upstream raw materials:

3-azapentane-1,5-diamine

1-benzyl-3,5-pyrazoledicarbaldehyde

Downstream raw materials:

13,26-dibenzyl-3,6,9,12,13,16,19,22,25,26-decaazatricyclo-[22.2.1.1^11,14]-octacosa-1⁽²⁷⁾,11,14⁽²⁸⁾,24-tetraene

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