C₂₂H₂₅N₉

Base Information

• Chemical Name: C₂₂H₂₅N₉
• CAS No.: 1415635-12-9
• Molecular Formula: C₂₂H₂₅N₉
• Molecular Weight: 415.501
• Mol file: 1415635-12-9.mol

Synonyms:C₂₂H₂₅N₉

Chemical Property of C₂₂H₂₅N₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₂H₂₅N₉

There total 3 articles about C₂₂H₂₅N₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

histamine (51-45-6) + C17H17ClN6 (1415635-39-0) → C22H25N9 (1415635-12-9)

Guidance literature:

histamine; C₁₇H₁₇ClN₆; With hydrogenchloride; In diethyl ether; butan-1-ol; at 110 ℃; for 0.5h;

With potassium carbonate;

Reference yield:

C17H17ClN6O (1415635-36-7) → C22H25N9 (1415635-12-9)

Guidance literature:

Multi-step reaction with 3 steps

1: ammonium formate / palladium-on-charcoal / water; tetrahydrofuran / 0.5 h / Inert atmosphere; Reflux

2: N-ethyl-N,N-diisopropylamine; trichlorophosphate / 6 h / 75 °C

3: hydrogenchloride / butan-1-ol; diethyl ether / 0.5 h / 110 °C

With hydrogenchloride; ammonium formate; N-ethyl-N,N-diisopropylamine; trichlorophosphate; palladium-on-charcoal; In tetrahydrofuran; diethyl ether; water; butan-1-ol;

Reference yield:

C17H18N6O (1415635-38-9) → C22H25N9 (1415635-12-9)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; trichlorophosphate / 6 h / 75 °C

2: hydrogenchloride / butan-1-ol; diethyl ether / 0.5 h / 110 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In diethyl ether; butan-1-ol;

upstream raw materials:

histamine

C₁₇H₁₇ClN₆

C₁₇H₁₇ClN₆O

C₁₇H₁₈N₆O

Refernces