ethyl 3-anilino-5-deoxy-2,3-O-isopropylidene-α-D-lyxo-furanoside

Base Information

Chemical Name:ethyl 3-anilino-5-deoxy-2,3-O-isopropylidene-α-D-lyxo-furanoside
CAS No.:228863-00-1
Molecular Formula:C₁₆H₂₃NO₄
Molecular Weight:293.363
Hs Code.:

Synonyms:ethyl 3-anilino-5-deoxy-2,3-O-isopropylidene-α-D-lyxo-furanoside

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Chemical Property of ethyl 3-anilino-5-deoxy-2,3-O-isopropylidene-α-D-lyxo-furanoside

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Technology Process of ethyl 3-anilino-5-deoxy-2,3-O-isopropylidene-α-D-lyxo-furanoside

There total 3 articles about ethyl 3-anilino-5-deoxy-2,3-O-isopropylidene-α-D-lyxo-furanoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 62-53-3
aniline

: 228862-99-5
ethyl 2,3-O-isopropylidene-α-D-lyxo-pentodialdo-1,4-furanoside

: 228863-00-1
ethyl 3-anilino-5-deoxy-2,3-O-isopropylidene-α-D-lyxo-furanoside

Guidance literature:: With 3 A molecular sieve; sodium cyanoborohydride; In methanol; at 20 ℃; for 2h; pH=6;
DOI:10.1016/S0008-6215(98)00313-9

Reference yield:

: 14131-84-1
2,3:5,6-di-O-isopropylidene-α-D-mannofuranose

: 228863-00-1
ethyl 3-anilino-5-deoxy-2,3-O-isopropylidene-α-D-lyxo-furanoside

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / silver(I) oxide / dimethylformamide / 24 h / 20 °C

2: 88 percent / periodic acid / diethyl ether / 12 h / 20 °C

3: 60 percent / 3A molecular sieves; sodium cyanoborohydride / methanol / 2 h / 20 °C / pH 6

With 3 A molecular sieve; sodium cyanoborohydride; periodic acid; silver(l) oxide; In methanol; diethyl ether; N,N-dimethyl-formamide; 1: Etherification / 2: Oxidation / 3: Reduction;
DOI:10.1016/S0008-6215(98)00313-9

Reference yield:

: 228862-98-4
ethyl 2,3-O-isopropylidene-α-D-mannofuranoside

: 228863-00-1
ethyl 3-anilino-5-deoxy-2,3-O-isopropylidene-α-D-lyxo-furanoside

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / sodium metaperiodate / H₂O / 0.5 h / 10 - 12 °C

2: 60 percent / 3A molecular sieves; sodium cyanoborohydride / methanol / 2 h / 20 °C / pH 6

With sodium periodate; 3 A molecular sieve; sodium cyanoborohydride; In methanol; water; 1: Oxidation / 2: Reduction;
DOI:10.1016/S0008-6215(98)00313-9