C₂₅H₃₂N₂O₇

Base Information

Chemical Name:C₂₅H₃₂N₂O₇
CAS No.:873676-51-8
Molecular Formula:C₂₅H₃₂N₂O₇
Molecular Weight:472.538
Hs Code.:

C<sub>25</sub>H<sub>32</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₂₅H₃₂N₂O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₂N₂O₇

Chemical Property:

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Technology Process of C₂₅H₃₂N₂O₇

There total 10 articles about C₂₅H₃₂N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 873676-50-7
C₂₆H₃₄N₂O₇

: 873676-51-8
C₂₅H₃₂N₂O₇

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; water; at 0 - 20 ℃;
DOI:10.1002/anie.200501553

Reference yield:

: 3,4-dihydroxy-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester

: 873676-51-8
C₂₅H₃₂N₂O₇

Guidance literature:: Multi-step reaction with 8 steps

1: magnesium sulfate; p-toluenesulfonic acid monohydrate / CH₂Cl₂ / 0 - 20 °C

2: 100 percent / HCl / dioxane / 1 h / 20 °C

3: 76 percent / HATU; ethyldiisopropylamine / CH₂Cl₂ / 18 h / 0 - 20 °C

4: 100 percent / HCl / dioxane; ethyl acetate / 20 °C

5: HATU; ethyldiisopropylamine / CH₂Cl₂ / 0 - 20 °C

6: 100 percent / hydrogen / palladium on carbon / ethyl acetate; ethanol / 16 h / 20 °C

7: 72 percent / 1,1'-(azodicarbonyl)dipiperidine; triphenylphosphane / CH₂Cl₂ / 24 h / 20 °C

8: lithium hydroxide / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

With hydrogenchloride; lithium hydroxide; hydrogen; magnesium sulfate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 1,1'-azodicarbonyl-dipiperidine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; ethyl acetate; 7: Mitsunobu reaction;
DOI:10.1002/anie.200501553

Reference yield:

: 873676-44-9
(2S,3aR,4S,6aS)-2-(3-Benzyloxy-propyl)-tetrahydro-[1,3]dioxolo[4,5-c]pyrrole-4,5-dicarboxylic acid 5-tert-butyl ester 4-methyl ester

: 873676-51-8
C₂₅H₃₂N₂O₇

Guidance literature:: Multi-step reaction with 7 steps

1: 100 percent / HCl / dioxane / 1 h / 20 °C

2: 76 percent / HATU; ethyldiisopropylamine / CH₂Cl₂ / 18 h / 0 - 20 °C

3: 100 percent / HCl / dioxane; ethyl acetate / 20 °C

4: HATU; ethyldiisopropylamine / CH₂Cl₂ / 0 - 20 °C

5: 100 percent / hydrogen / palladium on carbon / ethyl acetate; ethanol / 16 h / 20 °C

6: 72 percent / 1,1'-(azodicarbonyl)dipiperidine; triphenylphosphane / CH₂Cl₂ / 24 h / 20 °C

7: lithium hydroxide / tetrahydrofuran; methanol; H₂O / 0 - 20 °C

With hydrogenchloride; lithium hydroxide; hydrogen; N-ethyl-N,N-diisopropylamine; triphenylphosphine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 1,1'-azodicarbonyl-dipiperidine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; ethyl acetate; 6: Mitsunobu reaction;
DOI:10.1002/anie.200501553