N-benzoyl-N'-<5-<2-(3,5-dicarboethoxy-2,6-dimethyl-1,4-dihydropyridin-4-yl)phenoxy>pentyl>thiourea

Base Information

Chemical Name:N-benzoyl-N'-<5-<2-(3,5-dicarboethoxy-2,6-dimethyl-1,4-dihydropyridin-4-yl)phenoxy>pentyl>thiourea
CAS No.:153506-45-7
Molecular Formula:C₃₂H₃₉N₃O₆S
Molecular Weight:593.744
Hs Code.:

Synonyms:N-benzoyl-N'-<5-<2-(3,5-dicarboethoxy-2,6-dimethyl-1,4-dihydropyridin-4-yl)phenoxy>pentyl>thiourea

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Chemical Property of N-benzoyl-N'-<5-<2-(3,5-dicarboethoxy-2,6-dimethyl-1,4-dihydropyridin-4-yl)phenoxy>pentyl>thiourea

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Technology Process of N-benzoyl-N'-<5-<2-(3,5-dicarboethoxy-2,6-dimethyl-1,4-dihydropyridin-4-yl)phenoxy>pentyl>thiourea

There total 5 articles about N-benzoyl-N'-<5-<2-(3,5-dicarboethoxy-2,6-dimethyl-1,4-dihydropyridin-4-yl)phenoxy>pentyl>thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 532-55-8
Benzoyl isothiocyanate

: 153607-47-7
VUF 4587

: 153506-45-7
N-benzoyl-N'-<5-<2-(3,5-dicarboethoxy-2,6-dimethyl-1,4-dihydropyridin-4-yl)phenoxy>pentyl>thiourea

Guidance literature:: In dichloromethane; for 4h;
DOI:10.1016/0223-5234(93)90048-J

Reference yield:

: 954-81-4
N-(5-bromopentyl)phthalimide

: 153506-45-7
N-benzoyl-N'-<5-<2-(3,5-dicarboethoxy-2,6-dimethyl-1,4-dihydropyridin-4-yl)phenoxy>pentyl>thiourea

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / K₂CO₃ / dimethylformamide / 5 h / 110 °C

2: 1.) gl. acetic aciid, benzylamine / 1,) EtOH, reflux, 3 h, 2.) EtOH, reflux, overnight

3: 77 percent / hydrazine monohydrate / ethanol / 6 h / Heating

4: 51 percent / CH₂Cl₂ / 4 h

With potassium carbonate; hydrazine hydrate; acetic acid; benzylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(93)90048-J

Reference yield:

: 90-02-8
salicylaldehyde

: 153506-45-7
N-benzoyl-N'-<5-<2-(3,5-dicarboethoxy-2,6-dimethyl-1,4-dihydropyridin-4-yl)phenoxy>pentyl>thiourea

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / K₂CO₃ / dimethylformamide / 5 h / 110 °C

2: 1.) gl. acetic aciid, benzylamine / 1,) EtOH, reflux, 3 h, 2.) EtOH, reflux, overnight

3: 77 percent / hydrazine monohydrate / ethanol / 6 h / Heating

4: 51 percent / CH₂Cl₂ / 4 h

With potassium carbonate; hydrazine hydrate; acetic acid; benzylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(93)90048-J