3'-[2-(benzyloxy)-2-oxoethyl]-1,1'-biphenyl-2-yl 3,4,5-trihydroxybenzoate

Base Information

Chemical Name:3'-[2-(benzyloxy)-2-oxoethyl]-1,1'-biphenyl-2-yl 3,4,5-trihydroxybenzoate
CAS No.:1026692-25-0
Molecular Formula:C₂₈H₂₂O₇
Molecular Weight:470.478
Hs Code.:

Synonyms:3'-[2-(benzyloxy)-2-oxoethyl]-1,1'-biphenyl-2-yl 3,4,5-trihydroxybenzoate

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Chemical Property of 3'-[2-(benzyloxy)-2-oxoethyl]-1,1'-biphenyl-2-yl 3,4,5-trihydroxybenzoate

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Technology Process of 3'-[2-(benzyloxy)-2-oxoethyl]-1,1'-biphenyl-2-yl 3,4,5-trihydroxybenzoate

There total 10 articles about 3'-[2-(benzyloxy)-2-oxoethyl]-1,1'-biphenyl-2-yl 3,4,5-trihydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 934176-16-6
3'-[2-(benzyloxy)-2-oxoethyl]-1,1'-biphenyl-2-yl 3,4,5-tris(acetyloxy) benzoate

: 1026692-25-0
3'-[2-(benzyloxy)-2-oxoethyl]-1,1'-biphenyl-2-yl 3,4,5-trihydroxybenzoate

Guidance literature:: With ammonium hydroxide; In acetone; at 20 ℃; for 0.25h;
DOI:10.1021/jm060536g

Reference yield:

: 1025884-50-7
benzyl [2'-(tetrahydro-2H-pyran-2-yloxy)-1,1'-biphenyl-3-yl]-acetate

: 1026692-25-0
3'-[2-(benzyloxy)-2-oxoethyl]-1,1'-biphenyl-2-yl 3,4,5-trihydroxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 mg / pTsOH*H₂O / methanol / 2 h / 40 °C

2: 64 percent / Et₃N / CH₂Cl₂ / 0.58 h / 20 °C

3: aq. NH₃ / acetone / 0.25 h / 20 °C

With ammonium hydroxide; triethylamine; toluene-4-sulfonic acid; In methanol; dichloromethane; acetone;
DOI:10.1021/jm060536g

Reference yield:

: 4203-50-3
2-phenoxytetrahydropyran

: 1026692-25-0
3'-[2-(benzyloxy)-2-oxoethyl]-1,1'-biphenyl-2-yl 3,4,5-trihydroxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.75 h / -78 - 20 °C

1.2: triisopropyl borate / hexane; tetrahydrofuran / -78 - 20 °C

2.1: aq. Na₂CO₃ / tetrakis(triphenylphosphine)-palladium ⁽⁰⁾ / toluene / 2 h / 100 °C

3.1: 88 mg / pTsOH*H₂O / methanol / 2 h / 40 °C

4.1: 64 percent / Et₃N / CH₂Cl₂ / 0.58 h / 20 °C

5.1: aq. NH₃ / acetone / 0.25 h / 20 °C

With ammonium hydroxide; n-butyllithium; sodium carbonate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; acetone; toluene; 2.1: Suzuki reaction;
DOI:10.1021/jm060536g