3-(2-methoxy-3-methylthio-4-(trifluoromethyl)benzoyloxy)-cyclohex-2-enone

Base Information

Chemical Name:3-(2-methoxy-3-methylthio-4-(trifluoromethyl)benzoyloxy)-cyclohex-2-enone
CAS No.:1262515-33-2
Molecular Formula:C₁₆H₁₅F₃O₄S
Molecular Weight:360.354
Hs Code.:

Synonyms:3-(2-methoxy-3-methylthio-4-(trifluoromethyl)benzoyloxy)-cyclohex-2-enone

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Chemical Property of 3-(2-methoxy-3-methylthio-4-(trifluoromethyl)benzoyloxy)-cyclohex-2-enone

Chemical Property:

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Technology Process of 3-(2-methoxy-3-methylthio-4-(trifluoromethyl)benzoyloxy)-cyclohex-2-enone

There total 6 articles about 3-(2-methoxy-3-methylthio-4-(trifluoromethyl)benzoyloxy)-cyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1262652-16-3
2-methoxy-3-(methylsulfanyl)-4-(trifluoromethyl)benzoic acid

: 504-02-9
1,3-cylohexanedione

: 1262515-33-2
3-(2-methoxy-3-methylthio-4-(trifluoromethyl)benzoyloxy)-cyclohex-2-enone

Guidance literature:: 2-methoxy-3-(methylsulfanyl)-4-(trifluoromethyl)benzoic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; for 0.166667h; Reflux;

1,3-cylohexanedione; With triethylamine; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 401-80-9
3-fluoro-trifluoromethylbenzene

: 1262515-33-2
3-(2-methoxy-3-methylthio-4-(trifluoromethyl)benzoyloxy)-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 6 steps

1.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / 3 h / -78 - -65 °C / Inert atmosphere

2.2: -78 - 20 °C

3.1: sulfuric acid / Reflux

4.1: methanol / 6 h / Reflux

5.1: sodium hydroxide; water / methanol / 4 h / 20 °C

5.2: 20 °C / Cooling

6.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0.17 h / Reflux

6.2: 16 h / 20 °C

With methanol; n-butyllithium; oxalyl dichloride; sulfuric acid; water; diisopropylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane;

Reference yield:

: 709644-60-0
2-fluoro-6-trifluoromethyl-methylsulfanylbenzene

: 1262515-33-2
3-(2-methoxy-3-methylthio-4-(trifluoromethyl)benzoyloxy)-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 3 h / -78 - -65 °C / Inert atmosphere

1.2: -78 - 20 °C

2.1: sulfuric acid / Reflux

3.1: methanol / 6 h / Reflux

4.1: sodium hydroxide; water / methanol / 4 h / 20 °C

4.2: 20 °C / Cooling

5.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0.17 h / Reflux

5.2: 16 h / 20 °C

With methanol; n-butyllithium; oxalyl dichloride; sulfuric acid; water; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane;