Technology Process of C41H34
There total 3 articles about C41H34 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-methylphenylboronic acid; 4,4',4''-(ethene-1,1,2-triyl)tris(bromobenzene);
With
Aliquat 336; potassium carbonate;
In
water; toluene;
at 20 ℃;
for 0.75h;
Inert atmosphere;
With
tetrakis(triphenylphosphine) palladium(0);
In
water; toluene;
at 85 ℃;
for 16h;
Inert atmosphere;
DOI:10.1039/c0jm00229a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium tert-butylate / tetrahydrofuran / 2 h / Inert atmosphere
2.1: Aliquat 336; potassium carbonate / water; toluene / 0.75 h / 20 °C / Inert atmosphere
2.2: 16 h / 85 °C / Inert atmosphere
With
Aliquat 336; potassium tert-butylate; potassium carbonate;
In
tetrahydrofuran; water; toluene;
1.1: Wittig reaction / 2.1: Suzuki coupling / 2.2: Suzuki coupling;
DOI:10.1039/c0jm00229a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium tert-butylate / tetrahydrofuran / 2 h / Inert atmosphere
2.1: Aliquat 336; potassium carbonate / water; toluene / 0.75 h / 20 °C / Inert atmosphere
2.2: 16 h / 85 °C / Inert atmosphere
With
Aliquat 336; potassium tert-butylate; potassium carbonate;
In
tetrahydrofuran; water; toluene;
1.1: Wittig reaction / 2.1: Suzuki coupling / 2.2: Suzuki coupling;
DOI:10.1039/c0jm00229a
