C₃₂H₅₂N₂O₇S

Base Information

Chemical Name:C₃₂H₅₂N₂O₇S
CAS No.:1362119-77-4
Molecular Formula:C₃₂H₅₂N₂O₇S
Molecular Weight:608.84
Hs Code.:

C<sub>32</sub>H<sub>52</sub>N<sub>2</sub>O<sub>7</sub>S

Synonyms:C₃₂H₅₂N₂O₇S

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Chemical Property of C₃₂H₅₂N₂O₇S

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Technology Process of C₃₂H₅₂N₂O₇S

There total 28 articles about C₃₂H₅₂N₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1362120-15-7
C₃₂H₅₀N₂O₇S

: 1362119-77-4
C₃₂H₅₂N₂O₇S

: 1362120-03-3
C₃₂H₅₂N₂O₇S

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h; optical yield given as %de;
DOI:10.1021/ol300342n

Reference yield:

: C₁₄H₂₅NO₃

: 1362119-77-4
C₃₂H₅₂N₂O₇S

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene-4-sulfonic acid / water; acetone / 0.33 h

2.1: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 2.5 h

3.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 3 h / -20 °C

3.2: 3.5 h / -20 - 20 °C

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

4.2: 2 h / -78 °C

5.1: methanol; lithium borohydride / tetrahydrofuran / 2.67 h / 0 - 20 °C

6.1: tributylphosphine / tetrahydrofuran / 12.5 h / 0 - 20 °C

7.1: ammonium molybdate; dihydrogen peroxide / ethanol; water / 12 h

8.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.02 h / -78 °C

8.2: 0.33 h / -78 °C

9.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2.25 h / 0 - 20 °C

10.1: sodium tetrahydroborate / methanol / 1 h / 20 °C

With methanol; sodium chlorite; sodium tetrahydroborate; lithium borohydride; ammonium molybdate; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; tributylphosphine; dihydrogen peroxide; sodium hexamethyldisilazane; pivaloyl chloride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; acetone; tert-butyl alcohol; 2.1: Pinnick oxidation;
DOI:10.1021/ol300342n

Reference yield:

: 202926-14-5
tert-butyl hex-5-en-1-ylcarbamate

: 1362119-77-4
C₃₂H₅₂N₂O₇S

Guidance literature:: Multi-step reaction with 3 steps

1.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 5 h / 20 °C

2.1: (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether / methanol; 1,2-dichloro-ethane / 240 h / -25 °C

3.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.02 h / -78 °C

3.2: 0.33 h / -78 °C

With Hoveyda-Grubbs catalyst second generation; (R)-(-)-α,α-bis[3,5-bis(trifluoromethyl)phenyl]-2-pyrrolidinemethanoltrimethylsilyl ether; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dichloromethane; 1,2-dichloro-ethane; 2.1: intramolecular Michael addition;
DOI:10.1021/ol300342n