benzyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanate

Base Information

Chemical Name:benzyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanate
CAS No.:653595-58-5
Molecular Formula:C₂₀H₁₉F₃N₂O₉S
Molecular Weight:520.44
Hs Code.:

Synonyms:benzyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanate

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Technology Process of benzyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanate

There total 2 articles about benzyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 111339-17-4
benzyl 2-(trifluoromethyl)prop-2-enoate

: 2955-74-0
ethyl N-{[(4-nitrobenzene)sulfonyl]oxy}carbamate

: 653595-58-5
benzyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanate

Guidance literature:: With calcium oxide; In dichloromethane; for 7h;
DOI:10.1021/ol0361554

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 653595-58-5
benzyl N-(ethoxycarbonyl)-N-[(4-nitrophenylsulfonyl)oxy]-2-aminomethyl-3,3,3-trifluoropropanate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: 90 percent / CaO / CH₂Cl₂ / 7 h

With pyridine; calcium oxide; In dichloromethane; 2: aza-Michael addition;
DOI:10.1021/ol0361554