(S)-N-acetyl-2,6-dimethyltyrosine

Base Information

Chemical Name:(S)-N-acetyl-2,6-dimethyltyrosine
CAS No.:1333148-31-4
Molecular Formula:C₁₃H₁₇NO₄
Molecular Weight:251.282
Hs Code.:

Synonyms:(S)-N-acetyl-2,6-dimethyltyrosine

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Chemical Property of (S)-N-acetyl-2,6-dimethyltyrosine

Chemical Property:

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Technology Process of (S)-N-acetyl-2,6-dimethyltyrosine

There total 5 articles about (S)-N-acetyl-2,6-dimethyltyrosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 1333148-31-4
(S)-N-acetyl-2,6-dimethyltyrosine

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; potassium iodate; potassium iodide / methanol; water / 0 - 20 °C / Large scale reaction

2.1: pyridine / 10 °C

2.2: 39 - 55 °C / Large scale reaction

3.1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine

4.1: [Rh(1,5-COD)(S,S-Et-FerroTANE)]BF₄; hydrogen / ethyl acetate / 16 h / 60 °C / 3750.38 Torr

5.1: cobalt(II) chloride; sodium hydroxide / 35 °C / pH 8 - 10 / aq. phosphate buffer

With pyridine; hydrogenchloride; potassium iodate; [Rh(1,5-COD)(S,S-Et-FerroTANE)]BF₄; hydrogen; palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; potassium iodide; cobalt(II) chloride; sodium hydroxide; In methanol; water; ethyl acetate; 3.1: Heck reaction;
DOI:10.1021/op200065p

Reference yield:

: 80826-86-4
4-iodo-3,5-dimethylphenol

: 1333148-31-4
(S)-N-acetyl-2,6-dimethyltyrosine

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 10 °C

1.2: 39 - 55 °C / Large scale reaction

2.1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine

3.1: [Rh(1,5-COD)(S,S-Et-FerroTANE)]BF₄; hydrogen / ethyl acetate / 16 h / 60 °C / 3750.38 Torr

4.1: cobalt(II) chloride; sodium hydroxide / 35 °C / pH 8 - 10 / aq. phosphate buffer

With pyridine; [Rh(1,5-COD)(S,S-Et-FerroTANE)]BF₄; hydrogen; palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; cobalt(II) chloride; sodium hydroxide; In ethyl acetate; 2.1: Heck reaction;
DOI:10.1021/op200065p

Reference yield:

: 145235-84-3
4-iodo-3,5-dimethylphenyl acetate

: 1333148-31-4
(S)-N-acetyl-2,6-dimethyltyrosine

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine

2: [Rh(1,5-COD)(S,S-Et-FerroTANE)]BF₄; hydrogen / ethyl acetate / 16 h / 60 °C / 3750.38 Torr

3: cobalt(II) chloride; sodium hydroxide / 35 °C / pH 8 - 10 / aq. phosphate buffer

With [Rh(1,5-COD)(S,S-Et-FerroTANE)]BF₄; hydrogen; palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; cobalt(II) chloride; sodium hydroxide; In ethyl acetate; 1: Heck reaction;
DOI:10.1021/op200065p