dithiocarbonic acid S-{1-[(3,5-dichloro-phenylcarbamoyl)-methyl]-5,5-dimethyl-4-oxo-hexyl} ester O-ethyl ester

Base Information

• Chemical Name: dithiocarbonic acid S-{1-[(3,5-dichloro-phenylcarbamoyl)-methyl]-5,5-dimethyl-4-oxo-hexyl} ester O-ethyl ester
• CAS No.: 869667-18-5
• Molecular Formula: C₁₉H₂₅Cl₂NO₃S₂
• Molecular Weight: 450.45

Synonyms:dithiocarbonic acid S-{1-[(3,5-dichloro-phenylcarbamoyl)-methyl]-5,5-dimethyl-4-oxo-hexyl} ester O-ethyl ester

Chemical Property of dithiocarbonic acid S-{1-[(3,5-dichloro-phenylcarbamoyl)-methyl]-5,5-dimethyl-4-oxo-hexyl} ester O-ethyl ester

Chemical Property:

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Technology Process of dithiocarbonic acid S-{1-[(3,5-dichloro-phenylcarbamoyl)-methyl]-5,5-dimethyl-4-oxo-hexyl} ester O-ethyl ester

There total 2 articles about dithiocarbonic acid S-{1-[(3,5-dichloro-phenylcarbamoyl)-methyl]-5,5-dimethyl-4-oxo-hexyl} ester O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

but-3-enoic acid (3,5-dichloro-phenyl)-amide (869667-16-3) + O-ethyl S-(3,3-dimethyl-2-oxo-butyl) dithiocarbonate (82721-84-4) → dithiocarbonic acid S-{1-[(3,5-dichloro-phenylcarbamoyl)-methyl]-5,5-dimethyl-4-oxo-hexyl} ester O-ethyl ester (869667-18-5)

Guidance literature:

With dilauryl peroxide; In 1,2-dichloro-ethane; Heating;

DOI:10.1016/j.tetlet.2005.09.006

Reference yield:

3,5-Dichloroaniline (626-43-7) → dithiocarbonic acid S-{1-[(3,5-dichloro-phenylcarbamoyl)-methyl]-5,5-dimethyl-4-oxo-hexyl} ester O-ethyl ester (869667-18-5)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / 20 °C

2: 79 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; In dichloromethane; 1,2-dichloro-ethane;

DOI:10.1016/j.tetlet.2005.09.006

Reference yield: 56.0%

dithiocarbonic acid S-{1-[(3,5-dichloro-phenylcarbamoyl)-methyl]-5,5-dimethyl-4-oxo-hexyl} ester O-ethyl ester (869667-18-5) → 7,7-dimethyl-6-oxo-octanoic acid (3,5-dichloro-phenyl)-amide + 5,7-dichloro-4-(4,4-dimethyl-3-oxo-pentyl)-3,4-dihydro-1H-quinolin-2-one

Guidance literature:

With dilauryl peroxide; In chlorobenzene; Heating;

DOI:10.1016/j.tetlet.2005.09.006

upstream raw materials:

but-3-enoic acid (3,5-dichloro-phenyl)-amide

O-ethyl S-(3,3-dimethyl-2-oxo-butyl) dithiocarbonate

3,5-Dichloroaniline

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