methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-α-D-manno-2,4-nonudiulopyranosid]onate

Base Information

Chemical Name:methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-α-D-manno-2,4-nonudiulopyranosid]onate
CAS No.:1241906-68-2
Molecular Formula:C₂₉H₃₁ClF₂N₂O₉
Molecular Weight:625.023
Hs Code.:

Synonyms:methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-α-D-manno-2,4-nonudiulopyranosid]onate

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Chemical Property of methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-α-D-manno-2,4-nonudiulopyranosid]onate

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Technology Process of methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-α-D-manno-2,4-nonudiulopyranosid]onate

There total 1 articles about methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-α-D-manno-2,4-nonudiulopyranosid]onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1241906-47-7
methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-galacto-2-nonulopyranosid]onate

: 1241906-68-2
methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-α-D-manno-2,4-nonudiulopyranosid]onate

Guidance literature:: With dipyridinium dichromate; acetic anhydride; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1016/j.carres.2010.03.010

Reference yield: 36.0%

: 1241906-68-2
methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-α-D-manno-2,4-nonudiulopyranosid]onate

: 1241906-71-7
methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-D-glycero-α-D-talo-nonulopyranosid]onate

Guidance literature:: With borane-ammonia complex; In methanol; at 0 ℃; for 2h;
DOI:10.1016/j.carres.2010.03.010

Reference yield:

: 1241906-68-2
methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-α-D-manno-2,4-nonudiulopyranosid]onate

: 917-54-4
methyllithium

: C₃₀H₃₅ClF₂N₂O₉

Guidance literature:: methyllithium; With zirconium(IV) chloride; In tetrahydrofuran; hexane; at -54 - 0 ℃;

methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-7,8-O-isopropylidene-α-D-manno-2,4-nonudiulopyranosid]onate; In tetrahydrofuran; hexane; at -78 - 0 ℃;

With ammonium chloride; In tetrahydrofuran; hexane; at 0 ℃;
DOI:10.1016/j.carres.2010.03.010