2,2'-anhydro-3',4'-didehydro-3'-deoxy-5'-O-trityl-2',3'-secouridine

Base Information

• Chemical Name: 2,2'-anhydro-3',4'-didehydro-3'-deoxy-5'-O-trityl-2',3'-secouridine
• CAS No.: 212792-49-9
• Molecular Formula: C₂₈H₂₄N₂O₄
• Molecular Weight: 452.51

Synonyms:2,2'-anhydro-3',4'-didehydro-3'-deoxy-5'-O-trityl-2',3'-secouridine

Chemical Property of 2,2'-anhydro-3',4'-didehydro-3'-deoxy-5'-O-trityl-2',3'-secouridine

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Technology Process of 2,2'-anhydro-3',4'-didehydro-3'-deoxy-5'-O-trityl-2',3'-secouridine

There total 1 articles about 2,2'-anhydro-3',4'-didehydro-3'-deoxy-5'-O-trityl-2',3'-secouridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.8%

2',3'-dideoxy-2',3'-dibromo-5'-O-trityl-2',3'-secouridine (101527-48-4) → 2,2'-anhydro-3',4'-didehydro-3'-deoxy-5'-O-trityl-2',3'-secouridine (212792-49-9)

Guidance literature:

With potassium fluoride; In N,N-dimethyl-formamide; at 95 - 100 ℃; for 17h;

DOI:10.1080/07328319808003475

Reference yield: 84.0%

2,2'-anhydro-3',4'-didehydro-3'-deoxy-5'-O-trityl-2',3'-secouridine (212792-49-9) → 2'-chloro-3',4'-didehydro-2',3'-dideoxy-5'-O-trityl-2',3'-secouridine (212792-53-5)

Guidance literature:

With pyridine hydrochloride; In N,N-dimethyl-formamide; at 60 ℃; for 1h;

DOI:10.1080/07328319808003475

Reference yield: 83.7%

2,2'-anhydro-3',4'-didehydro-3'-deoxy-5'-O-trityl-2',3'-secouridine (212792-49-9) → 3',4'-didehydro-2',3'-dideoxy-2'-iodo-5'-O-trityl-2',3'-secouridine (212792-57-9)

Guidance literature:

With pyridine hydroiodide; In N,N-dimethyl-formamide; for 19h; Ambient temperature;

DOI:10.1080/07328319808003475

upstream raw materials:

2',3'-dideoxy-2',3'-dibromo-5'-O-trityl-2',3'-secouridine

Downstream raw materials:

3',4'-didehydro-3'-deoxy-5'-O-trityl-2',3'-secouridine

2'-chloro-3',4'-didehydro-2',3'-dideoxy-5'-O-trityl-2',3'-secouridine

2'-bromo-3',4'-didehydro-2',3'-dideoxy-5'-O-trityl-2',3'-secouridine

3',4'-didehydro-2',3'-dideoxy-2'-iodo-5'-O-trityl-2',3'-secouridine

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