Technology Process of C29H32N6O
There total 8 articles about C29H32N6O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
o-toluidine;
With
sodium hydride;
In
1,4-dioxane;
for 1.5h;
C28H29N5O2;
In
1,4-dioxane;
at 20 ℃;
for 18h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: thiophene; hydrogen / platinum on carbon / tetrahydrofuran; methanol / 20 °C
2.1: sodium hydrogencarbonate / acetonitrile / 0.25 h / 20 °C / cooled on a water bath
3.1: hydrogen / palladium 10% on activated carbon / methanol
4.1: tetrahydrofuran / 18 h / 55 °C
5.1: sodium hydride / 1,4-dioxane / 1.5 h
5.2: 18 h / 20 °C
With
thiophene; hydrogen; sodium hydride; sodium hydrogencarbonate;
palladium 10% on activated carbon; platinum on carbon;
In
tetrahydrofuran; 1,4-dioxane; methanol; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydrogencarbonate / acetonitrile / 0.25 h / 20 °C / cooled on a water bath
2.1: hydrogen / palladium 10% on activated carbon / methanol
3.1: tetrahydrofuran / 18 h / 55 °C
4.1: sodium hydride / 1,4-dioxane / 1.5 h
4.2: 18 h / 20 °C
With
hydrogen; sodium hydride; sodium hydrogencarbonate;
palladium 10% on activated carbon;
In
tetrahydrofuran; 1,4-dioxane; methanol; acetonitrile;