ethyl 3-[2-(1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbonyl) hydrazono]butanoate

Base Information

Chemical Name:ethyl 3-[2-(1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbonyl) hydrazono]butanoate
CAS No.:1400701-18-9
Molecular Formula:C₂₂H₂₄N₆O₅
Molecular Weight:452.47
Hs Code.:

Synonyms:ethyl 3-[2-(1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbonyl) hydrazono]butanoate

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Chemical Property of ethyl 3-[2-(1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbonyl) hydrazono]butanoate

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Technology Process of ethyl 3-[2-(1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbonyl) hydrazono]butanoate

There total 6 articles about ethyl 3-[2-(1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbonyl) hydrazono]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1400700-92-6
C₁₆H₁₆N₆O₃

: 141-97-9
ethyl acetoacetate

: 1400701-18-9
ethyl 3-[2-(1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbonyl) hydrazono]butanoate

Guidance literature:: for 5h; Reflux;
DOI:10.1016/j.ejmech.2012.06.048

Reference yield:

: 1400700-86-8
C₁₈H₁₈N₄O₄

: 1400701-18-9
ethyl 3-[2-(1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbonyl) hydrazono]butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 5 h / 20 °C

2: 5 h / Reflux

With hydrazine hydrate; In ethanol;
DOI:10.1016/j.ejmech.2012.06.048

Reference yield:

: 565178-04-3
C₁₄H₁₂N₄O

: 1400701-18-9
ethyl 3-[2-(1,6-dioxo-5-phenyl-1,2,5,6,8,9,10,10a,-octahydropyrimido[5,4-e]pyrrolo[1,2-c]pyrimidine-3-carbonyl) hydrazono]butanoate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate / ethanol

2: benzene / 3 h / 20 °C

3: 2 h / Reflux

4: hydrazine hydrate / ethanol / 5 h / 20 °C

5: 5 h / Reflux

With sodium tetrahydroborate; hydrazine hydrate; In ethanol; benzene;
DOI:10.1016/j.ejmech.2012.06.048