C₁₉H₂₄O₂Si

Base Information

Chemical Name:C₁₉H₂₄O₂Si
CAS No.:1373401-90-1
Molecular Formula:C₁₉H₂₄O₂Si
Molecular Weight:312.484
Hs Code.:

C<sub>19</sub>H<sub>24</sub>O<sub>2</sub>Si

Synonyms:C₁₉H₂₄O₂Si

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Chemical Property of C₁₉H₂₄O₂Si

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Technology Process of C₁₉H₂₄O₂Si

There total 1 articles about C₁₉H₂₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 1373401-90-1
C₁₉H₂₄O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1.08 h / Cooling with acetone-dry ice; Inert atmosphere

1.2: 1.83 h / Inert atmosphere

1.3: Inert atmosphere

2.1: methanol; dichloromethane / 12.5 h / 5 °C / Cooling with ice-water; Inert atmosphere

2.2: 0.42 h / Inert atmosphere

2.3: 0.92 h / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; methanol; hexane; dichloromethane;

Reference yield: 94.0%

: 108-22-5
Isopropenyl acetate

: 1373401-90-1
C₁₉H₂₄O₂Si

: 1373390-80-7
C₂₁H₂₆O₃Si

Guidance literature:: C₁₉H₂₄O₂Si; With triethylamine; Inert atmosphere;

Isopropenyl acetate; at 23 ℃; for 20h; Inert atmosphere;

Reference yield:

: 1373401-90-1
C₁₉H₂₄O₂Si

: 1373390-81-8
C₁₉H₂₂OSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / Inert atmosphere

1.2: Lipase Amano "PS" IM / 20 h / 23 °C / Inert atmosphere

2.1: water; ammonium formate / N,N-dimethyl-formamide / 0.67 h / 23 °C / Inert atmosphere

2.2: 16 h / 23 °C / Inert atmosphere

With water; ammonium formate; triethylamine; In N,N-dimethyl-formamide;