bis-(4,4,5,5,6,6,7,7,7-nonafluoro-heptyl)-thiocarbamic acid O-(1-methyl-2-phenyl-ethyl) ester

Base Information

Chemical Name:bis-(4,4,5,5,6,6,7,7,7-nonafluoro-heptyl)-thiocarbamic acid O-(1-methyl-2-phenyl-ethyl) ester
CAS No.:910660-89-8
Molecular Formula:C₂₄H₂₃F₁₈NOS
Molecular Weight:715.49
Hs Code.:

bis-(4,4,5,5,6,6,7,7,7-nonafluoro-heptyl)-thiocarbamic acid <i>O</i>-(1-methyl-2-phenyl-ethyl) ester

Synonyms:bis-(4,4,5,5,6,6,7,7,7-nonafluoro-heptyl)-thiocarbamic acid O-(1-methyl-2-phenyl-ethyl) ester

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Chemical Property of bis-(4,4,5,5,6,6,7,7,7-nonafluoro-heptyl)-thiocarbamic acid O-(1-methyl-2-phenyl-ethyl) ester

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Technology Process of bis-(4,4,5,5,6,6,7,7,7-nonafluoro-heptyl)-thiocarbamic acid O-(1-methyl-2-phenyl-ethyl) ester

There total 3 articles about bis-(4,4,5,5,6,6,7,7,7-nonafluoro-heptyl)-thiocarbamic acid O-(1-methyl-2-phenyl-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 910660-81-0
C₁₅H₁₂ClF₁₈NS

: 698-87-3,14898-87-4
3-phenyl-2-propanol

: 910660-89-8
bis-(4,4,5,5,6,6,7,7,7-nonafluoro-heptyl)-thiocarbamic acid O-(1-methyl-2-phenyl-ethyl) ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2006.05.142

Reference yield:

: 910660-90-1
bis-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-thiocarbamic acid O-(1-methyl-2-phenyl-ethyl) ester

: 910660-89-8
bis-(4,4,5,5,6,6,7,7,7-nonafluoro-heptyl)-thiocarbamic acid O-(1-methyl-2-phenyl-ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / m-CPBA / CH₂Cl₂ / 1 h / -78 °C

2: 100 percent / NaH / tetrahydrofuran / 12 h / 20 °C

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2006.05.142

Reference yield:

: bis-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl)-thiocarbamic acid O-(1-methyl-2-phenyl-ethyl) ester

: 910660-89-8
bis-(4,4,5,5,6,6,7,7,7-nonafluoro-heptyl)-thiocarbamic acid O-(1-methyl-2-phenyl-ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / m-CPBA / CH₂Cl₂ / 1 h / -78 °C

2: 100 percent / NaH / tetrahydrofuran / 12 h / 20 °C

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2006.05.142