(2S,3R)-1-(benzyl(methyl)amino)-3-(3-methoxyphenyl)-2-methyl-3-pentanol

Base Information

Chemical Name:(2S,3R)-1-(benzyl(methyl)amino)-3-(3-methoxyphenyl)-2-methyl-3-pentanol
CAS No.:1353891-32-3
Molecular Formula:C₂₁H₂₉NO₂
Molecular Weight:327.467
Hs Code.:

Synonyms:(2S,3R)-1-(benzyl(methyl)amino)-3-(3-methoxyphenyl)-2-methyl-3-pentanol

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Chemical Property of (2S,3R)-1-(benzyl(methyl)amino)-3-(3-methoxyphenyl)-2-methyl-3-pentanol

Chemical Property:

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Technology Process of (2S,3R)-1-(benzyl(methyl)amino)-3-(3-methoxyphenyl)-2-methyl-3-pentanol

There total 5 articles about (2S,3R)-1-(benzyl(methyl)amino)-3-(3-methoxyphenyl)-2-methyl-3-pentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353891-28-7
(S)-3-(benzyl-methylamino)-2-methyl-1-(3-methoxy-phenyl)-propan-1-one

: 925-90-6
ethylmagnesium bromide

: 1353891-32-3
(2S,3R)-1-(benzyl(methyl)amino)-3-(3-methoxyphenyl)-2-methyl-3-pentanol

Guidance literature:: (S)-3-(benzyl-methylamino)-2-methyl-1-(3-methoxy-phenyl)-propan-1-one; ethylmagnesium bromide; In 2-methyltetrahydrofuran; at 10 - 35 ℃; Inert atmosphere;

With ammonium bisulphate; In 2-methyltetrahydrofuran; at 4 ℃;

Reference yield:

: 47235-20-1
3-(benzyl-methyl-amino)-2-methyl-1-(3-methoxy-phenyl)-propan-1-one

: 1353891-32-3
(2S,3R)-1-(benzyl(methyl)amino)-3-(3-methoxyphenyl)-2-methyl-3-pentanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: isopropyl alcohol / 50 h / 4 - 25 °C

2.1: sodium hydroxide / water / 4 - 25 °C / pH 10 - 12

3.1: 2-methyltetrahydrofuran / 10 - 35 °C / Inert atmosphere

3.2: 4 °C

With sodium hydroxide; In 2-methyltetrahydrofuran; water; isopropyl alcohol;

Reference yield:

: 103-67-3
benzyl-methyl-amine

: 1353891-32-3
(2S,3R)-1-(benzyl(methyl)amino)-3-(3-methoxyphenyl)-2-methyl-3-pentanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / acetonitrile; water / 10 - 65 °C

1.2: 0.5 h / pH 11 - 13

2.1: isopropyl alcohol / 50 h / 4 - 25 °C

3.1: sodium hydroxide / water / 4 - 25 °C / pH 10 - 12

4.1: 2-methyltetrahydrofuran / 10 - 35 °C / Inert atmosphere

4.2: 4 °C

With hydrogenchloride; sodium hydroxide; In 2-methyltetrahydrofuran; water; isopropyl alcohol; acetonitrile; 1.1: Mannich Reaction;