5,6,8,9-tetrahydro-7-phenyldibenzoxanthylium monofluoride

Base Information

• Chemical Name: 5,6,8,9-tetrahydro-7-phenyldibenzoxanthylium monofluoride
• CAS No.: 81454-10-6
• Molecular Formula: C₂₇H₂₁O*F
• Molecular Weight: 380.462
• Mol file: 81454-10-6.mol

Synonyms:5,6,8,9-tetrahydro-7-phenyldibenzoxanthylium monofluoride

Chemical Property of 5,6,8,9-tetrahydro-7-phenyldibenzoxanthylium monofluoride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 5,6,8,9-tetrahydro-7-phenyldibenzoxanthylium monofluoride

There total 1 articles about 5,6,8,9-tetrahydro-7-phenyldibenzoxanthylium monofluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3,4-dihydro-2-<α-(1,2,3,4-tetrahydro-1-oxo-2-naphthyl)-benzylidene>naphthalen-1(2H)-one (76192-29-5) → 5,6,8,9-tetrahydro-7-phenyldibenzoxanthylium monofluoride (81454-10-6)

Guidance literature:

With hydrogen fluoride; In toluene; at 25 ℃; for 12h;

DOI:10.1016/S0040-4020(01)98888-X

Reference yield: 89.0%

5,6,8,9-tetrahydro-7-phenyldibenzoxanthylium monofluoride (81454-10-6) + aniline (62-53-3) → 7,14-Diphenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium; fluoride (81454-21-9)

Guidance literature:

In ethanol; benzene; for 16h; Product distribution; Heating; reaction with various arylamines;

DOI:10.1016/S0040-4020(01)98888-X

Reference yield: 85.0%

4-chloro-aniline (106-47-8) + 5,6,8,9-tetrahydro-7-phenyldibenzoxanthylium monofluoride (81454-10-6) → 14-(4-Chloro-phenyl)-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium; fluoride (81454-22-0)

Guidance literature:

In ethanol; benzene; for 16h; Heating;

DOI:10.1016/S0040-4020(01)98888-X

upstream raw materials:

3,4-dihydro-2-<α-(1,2,3,4-tetrahydro-1-oxo-2-naphthyl)-benzylidene>naphthalen-1(2H)-one

Downstream raw materials:

14-(4-Chloro-phenyl)-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium; fluoride

7,14-Diphenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium; fluoride

14-(4-Bromo-phenyl)-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridinium; fluoride