L-(2β,3aα,8aα)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole

Base Information

• Chemical Name: L-(2β,3aα,8aα)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole
• CAS No.: 79465-82-0
• Molecular Formula: C₁₄H₁₆N₂O₄
• Molecular Weight: 276.292

Synonyms:L-(2β,3aα,8aα)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole

Chemical Property of L-(2β,3aα,8aα)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole

Chemical Property:

Purity/Quality:

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Technology Process of L-(2β,3aα,8aα)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole

There total 3 articles about L-(2β,3aα,8aα)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Nb-methoxycarbonyl-DL-tryptophan methyl ester (66377-68-2) → DL-(2β,3aα,8aα)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole (67811-38-5,79465-82-0,79465-87-5,136088-17-0,146235-39-4)

Guidance literature:

With phosphoric acid; for 3h; Ambient temperature;

DOI:10.1016/S0040-4020(01)92088-5

Reference yield:

Nb-methoxycarbonyl-DL-tryptophan methyl ester (66377-68-2) → DL-(2β,3aα,8aα)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole (67811-38-5,79465-82-0,79465-87-5,136088-17-0,146235-39-4) + DL-(2β,3aβ,8aβ)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole (67811-38-5,79465-82-0,79465-87-5,136088-17-0,146235-39-4)

Guidance literature:

With phosphoric acid; for 3h; Product distribution; Mechanism; Ambient temperature; variation of acids, reaction times and temperatures;

DOI:10.1016/S0040-4020(01)92088-5

Reference yield:

Nb-methoxycarbonyl-DL-tryptophan methyl ester (66377-68-2) → DL-(2β,3aα,8aα)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole (67811-38-5,79465-82-0,79465-87-5,136088-17-0,146235-39-4) + DL-(2β,3aβ,8aβ)-1,2,3,3a,8,8a-hexahydro-1,2-dimethoxycarbonylpyrrolo<2,3-b>indole (67811-38-5,79465-82-0,79465-87-5,136088-17-0,146235-39-4)

Guidance literature:

With phosphoric acid; for 3h; Product distribution; Mechanism; Ambient temperature; variation of acids, reaction times and temperatures;

DOI:10.1016/S0040-4020(01)92088-5

upstream raw materials:

N_b-methoxycarbonyl-DL-tryptophan methyl ester

Downstream raw materials:

dimethyl (2S,3aR,8aS)-8-benzenesulphonyl-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole-1,2-dicarboxylate

Dimethyl 8-<(4-methoxyphenyl)sulfonyl>-1,2(S),3,3a(R),8,8a(S)-hexahydropyrrolo<2,3-b>indole-1,2-dicarboxylate

C₂₃H₂₆N₂O₆S

C₄₅H₅₃N₅O₁₁S

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