C₅₆H₇₇N₅O₁₃Si₂

Base Information

Chemical Name:C₅₆H₇₇N₅O₁₃Si₂
CAS No.:1616784-17-8
Molecular Formula:C₅₆H₇₇N₅O₁₃Si₂
Molecular Weight:1084.42
Hs Code.:

C<sub>56</sub>H<sub>77</sub>N<sub>5</sub>O<sub>13</sub>Si<sub>2</sub>

Synonyms:C₅₆H₇₇N₅O₁₃Si₂

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Chemical Property of C₅₆H₇₇N₅O₁₃Si₂

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Technology Process of C₅₆H₇₇N₅O₁₃Si₂

There total 7 articles about C₅₆H₇₇N₅O₁₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1558008-06-2
5'-amino-5'-deoxy-2'-O-triisopropylsilyloxymethyluridine

: 1616784-15-6
C₃₇H₄₄N₂O₈Si

: 1616784-17-8
C₅₆H₇₇N₅O₁₃Si₂

Guidance literature:: With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1093/nar/gku235

Reference yield:

: 200011-14-9
1-[3-C-allyl-2,5-O-bis(tert-butyldimethylsilyl)-β-D-pentofuranosyl]-uracyl

: 1616784-17-8
C₅₆H₇₇N₅O₁₃Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid / tetrahydrofuran; water / 4 h / 0 °C

2.1: pyridine / 14 h / 0 - 20 °C

3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / 1,4-dioxane / 10 h / 20 °C

3.2: 12 h / 20 °C

4.1: sodium perchlorate; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 1 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol / dichloromethane / 12 h / 20 °C

With pyridine; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; sodium perchlorate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; tert-butyl alcohol;
DOI:10.1093/nar/gku235

Reference yield:

: triisopropyl-2-chloroethoxysilane

: 1616784-17-8
C₅₆H₇₇N₅O₁₃Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine; dibutyltin chloride / 1,2-dichloro-ethane / 1 h / 20 °C

1.2: 0.75 h / 80 °C

2.1: pyridine; hydrogen sulfide / water / 14 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; benzotriazol-1-ol / dichloromethane / 12 h / 20 °C

With pyridine; hydrogen sulfide; dibutyltin chloride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1093/nar/gku235