(-)-(4S)-1-benzyl-4-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-azetidine-2,3-dione

Base Information

Chemical Name:(-)-(4S)-1-benzyl-4-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-azetidine-2,3-dione
CAS No.:160527-44-6
Molecular Formula:C₁₅H₁₇NO₄
Molecular Weight:275.304
Hs Code.:

Synonyms:(-)-(4S)-1-benzyl-4-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-azetidine-2,3-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(4S)-1-benzyl-4-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-azetidine-2,3-dione

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Technology Process of (-)-(4S)-1-benzyl-4-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-azetidine-2,3-dione

There total 5 articles about (-)-(4S)-1-benzyl-4-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-azetidine-2,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-1-Benzyl-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-hydroxy-azetidin-2-one

: 160527-44-6
(-)-(4S)-1-benzyl-4-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-azetidine-2,3-dione

Guidance literature:: With phosphorus pentoxide; In dimethyl sulfoxide; for 24h; Ambient temperature;
DOI:10.1016/S0040-4039(00)77015-8

Reference yield:

: 131319-74-9
(R)-2,3-di-O-isoproylideneglyceraldehyde N-benzylimine

: 13831-31-7
Acetoxyacetyl chloride

: 160527-44-6
(-)-(4S)-1-benzyl-4-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-azetidine-2,3-dione

Guidance literature:: (R)-2,3-di-O-isoproylideneglyceraldehyde N-benzylimine; Acetoxyacetyl chloride; With triethylamine; In dichloromethane; at 20 ℃;

With sodium methylate; In methanol; at 0 ℃;

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 ℃; for 2h;
DOI:10.1002/1521-3765(20020816)8:16<3646::AID-CHEM3646>3.0.CO;2-M

Reference yield:

: C₁₅H₁₉NO₄

: 160527-44-6
(-)-(4S)-1-benzyl-4-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]-azetidine-2,3-dione

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1002/ejoc.200800521