N-(3-chlorophenethyl)-2,4,6-trimethyl-N-((3'-cyano-[1,1'-biphenyl]-4-yl)methyl)benzenesulfonamide

Base Information

• Chemical Name: N-(3-chlorophenethyl)-2,4,6-trimethyl-N-((3'-cyano-[1,1'-biphenyl]-4-yl)methyl)benzenesulfonamide
• CAS No.: 1613029-07-4
• Molecular Formula: C₃₁H₂₉ClN₂O₂S
• Molecular Weight: 529.102

Synonyms:N-(3-chlorophenethyl)-2,4,6-trimethyl-N-((3'-cyano-[1,1'-biphenyl]-4-yl)methyl)benzenesulfonamide

Chemical Property of N-(3-chlorophenethyl)-2,4,6-trimethyl-N-((3'-cyano-[1,1'-biphenyl]-4-yl)methyl)benzenesulfonamide

Chemical Property:

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Technology Process of N-(3-chlorophenethyl)-2,4,6-trimethyl-N-((3'-cyano-[1,1'-biphenyl]-4-yl)methyl)benzenesulfonamide

There total 2 articles about N-(3-chlorophenethyl)-2,4,6-trimethyl-N-((3'-cyano-[1,1'-biphenyl]-4-yl)methyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

N-(3-chlorophenethyl)-N-(4-iodobenzyl)-2,4,6-trimethylbenzenesulfonamide (1613028-99-1) + (3‐cyanophenyl)boronic acid (150255-96-2) → N-(3-chlorophenethyl)-2,4,6-trimethyl-N-((3'-cyano-[1,1'-biphenyl]-4-yl)methyl)benzenesulfonamide (1613029-07-4)

Guidance literature:

With palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine; In 1,4-dioxane; water; at 90 ℃; Inert atmosphere;

DOI:10.1016/j.bioorg.2021.105540

Reference yield:

→ N-(3-chlorophenethyl)-2,4,6-trimethyl-N-((3'-cyano-[1,1'-biphenyl]-4-yl)methyl)benzenesulfonamide (1613029-07-4)

Guidance literature:

With palladium diacetate; tris-(o-tolyl)phosphine; In 1,4-dioxane; at 120 ℃; Inert atmosphere;

Reference yield: 98.0%

N-(3-chlorophenethyl)-2,4,6-trimethyl-N-((3'-cyano-[1,1'-biphenyl]-4-yl)methyl)benzenesulfonamide (1613029-07-4) → N-((3'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-N-(3-chlorophenethyl)-2,4,6-trimethylbenzenesulfonamide

Guidance literature:

With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 120 ℃; for 12h;

DOI:10.1016/j.bioorg.2021.105540

upstream raw materials:

N-(3-chlorophenethyl)-N-(4-iodobenzyl)-2,4,6-trimethylbenzenesulfonamide

(3‐cyanophenyl)boronic acid

Downstream raw materials:

4'-((N-(3-chlorophenethyl)-2,4,6-trimethylphenylsulfonamido)methyl)-[1,1'-biphenyl]-3-carboxamide

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