6-benzyloxy-3-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-hydroxy-4-methoxyacetophenone

Base Information

Chemical Name:6-benzyloxy-3-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-hydroxy-4-methoxyacetophenone
CAS No.:169566-44-3
Molecular Formula:C₅₀H₅₀O₉
Molecular Weight:794.942
Hs Code.:

Synonyms:6-benzyloxy-3-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-hydroxy-4-methoxyacetophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-benzyloxy-3-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-hydroxy-4-methoxyacetophenone

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Technology Process of 6-benzyloxy-3-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-hydroxy-4-methoxyacetophenone

There total 5 articles about 6-benzyloxy-3-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-hydroxy-4-methoxyacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 10299-59-9
1‐(2‐(benzyloxy)‐6‐hydroxy‐4‐methoxyphenyl)ethan‐1‐one

: 89025-46-7
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl fluoride

: 169566-44-3
6-benzyloxy-3-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-hydroxy-4-methoxyacetophenone

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -70 - 20 ℃; for 5h; Molecular sieve;
DOI:10.1016/j.carres.2013.03.016

Reference yield: 81.0%

: 10299-59-9
1‐(2‐(benzyloxy)‐6‐hydroxy‐4‐methoxyphenyl)ethan‐1‐one

: 74808-09-6
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 169566-44-3
6-benzyloxy-3-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-hydroxy-4-methoxyacetophenone

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate;
DOI:10.1016/j.carres.2013.03.016

Reference yield: 15.0%

: 10299-59-9
1‐(2‐(benzyloxy)‐6‐hydroxy‐4‐methoxyphenyl)ethan‐1‐one

: 89025-46-7
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl fluoride

: 169566-44-3
6-benzyloxy-3-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-hydroxy-4-methoxyacetophenone

: 2-benzyloxy-6-hydroxy-4-methoxy-3-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)acetophenone

: 2-benzyloxy-4-methoxy-6-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)acetophenone

Guidance literature:: With 4 A molecular sieve; boron trifluoride diethyl etherate; In dichloromethane; at -20 - 20 ℃;
DOI:10.1246/bcsj.68.1379