7a-hydroperoxy-2-methyl-6-(4-methoxyphenyl)-3a,7a-dihydrofuro<3,2-b>pyran-5-one

Base Information

Chemical Name:7a-hydroperoxy-2-methyl-6-(4-methoxyphenyl)-3a,7a-dihydrofuro<3,2-b>pyran-5-one
CAS No.:83311-55-1
Molecular Formula:C₁₅H₁₄O₆
Molecular Weight:290.273
Hs Code.:

Synonyms:7a-hydroperoxy-2-methyl-6-(4-methoxyphenyl)-3a,7a-dihydrofuro<3,2-b>pyran-5-one

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Chemical Property of 7a-hydroperoxy-2-methyl-6-(4-methoxyphenyl)-3a,7a-dihydrofuro<3,2-b>pyran-5-one

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Technology Process of 7a-hydroperoxy-2-methyl-6-(4-methoxyphenyl)-3a,7a-dihydrofuro<3,2-b>pyran-5-one

There total 3 articles about 7a-hydroperoxy-2-methyl-6-(4-methoxyphenyl)-3a,7a-dihydrofuro<3,2-b>pyran-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 83307-77-1
(E)-2-(4-Methoxy-phenyl)-3-(5-methyl-furan-2-yl)-acrylic acid

: 83311-55-1
7a-hydroperoxy-2-methyl-6-(4-methoxyphenyl)-3a,7a-dihydrofuro<3,2-b>pyran-5-one

Guidance literature:: With air; 4,5,6,7-tetrachloro-2',4',5',7'-tetraiodofluorescein disodium salt; In methanol; for 20h; Ambient temperature; Irradiation;
DOI:10.1016/0040-4020(82)85121-1

Reference yield:

: 620-02-0
5-Methylfurfural

: 83311-55-1
7a-hydroperoxy-2-methyl-6-(4-methoxyphenyl)-3a,7a-dihydrofuro<3,2-b>pyran-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / triethylamine; acetic anhydride / 1.5 h / Heating

2: 70 percent / air, Bengal Rose / methanol / 20 h / Ambient temperature; Irradiation

With air; 4,5,6,7-tetrachloro-2',4',5',7'-tetraiodofluorescein disodium salt; In methanol; acetic anhydride; triethylamine;
DOI:10.1016/0040-4020(82)85121-1

Reference yield:

: 104-01-8
4-Methoxyphenylacetic acid

: 83311-55-1
7a-hydroperoxy-2-methyl-6-(4-methoxyphenyl)-3a,7a-dihydrofuro<3,2-b>pyran-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / triethylamine; acetic anhydride / 1.5 h / Heating

2: 70 percent / air, Bengal Rose / methanol / 20 h / Ambient temperature; Irradiation

With air; 4,5,6,7-tetrachloro-2',4',5',7'-tetraiodofluorescein disodium salt; In methanol; acetic anhydride; triethylamine;
DOI:10.1016/0040-4020(82)85121-1