2-(4-metossicarbonilfenil)-3-oxo-2,3-diidro-1,2-benzisotiazolo-1,1-diossido

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Chemical Name:2-(4-metossicarbonilfenil)-3-oxo-2,3-diidro-1,2-benzisotiazolo-1,1-diossido
CAS No.:102486-62-4
Molecular Formula:C₁₅H₁₁NO₅S
Molecular Weight:317.322
Hs Code.:

Synonyms:2-(4-metossicarbonilfenil)-3-oxo-2,3-diidro-1,2-benzisotiazolo-1,1-diossido

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Chemical Property of 2-(4-metossicarbonilfenil)-3-oxo-2,3-diidro-1,2-benzisotiazolo-1,1-diossido

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Technology Process of 2-(4-metossicarbonilfenil)-3-oxo-2,3-diidro-1,2-benzisotiazolo-1,1-diossido

There total 5 articles about 2-(4-metossicarbonilfenil)-3-oxo-2,3-diidro-1,2-benzisotiazolo-1,1-diossido which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: C₁₄H₁₂INO₄S

: 1864-94-4
phenyl formate

: 102486-62-4
2-(4-metossicarbonilfenil)-3-oxo-2,3-diidro-1,2-benzisotiazolo-1,1-diossido

Guidance literature:: With palladium diacetate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 80 ℃; for 18h; Schlenk technique; Inert atmosphere;
DOI:10.1055/s-0036-1588422

Reference yield: 70.0%

: 4322-93-4
Methyl 4-(3-oxobenzo[d]isothiazol-2(3H)-yl)benzoate

: 102486-62-4
2-(4-metossicarbonilfenil)-3-oxo-2,3-diidro-1,2-benzisotiazolo-1,1-diossido

Guidance literature:: With dihydrogen peroxide; In acetic acid; at 70 ℃; for 2h;

Reference yield:

: 19602-82-5
2,2'-dithiodibenzoic acid dichloride

: 102486-62-4
2-(4-metossicarbonilfenil)-3-oxo-2,3-diidro-1,2-benzisotiazolo-1,1-diossido

Guidance literature:: Multi-step reaction with 3 steps

1: Cl₂ / CCl₄ / Ambient temperature

2: 45 percent / pyridine / 0.33 h / 50 °C

3: 70 percent / 36percent H₂O₂ / acetic acid / 2 h / 70 °C

With dihydrogen peroxide; chlorine; In pyridine; tetrachloromethane; acetic acid;