(+/-)-2-(1-(methoxycarbonyl)-5-ethyl-2-methoxycyclohexa-2,5-dienyl)acetic acid

Base Information

Chemical Name:(+/-)-2-(1-(methoxycarbonyl)-5-ethyl-2-methoxycyclohexa-2,5-dienyl)acetic acid
CAS No.:881897-25-2
Molecular Formula:C₁₃H₁₈O₅
Molecular Weight:254.283
Hs Code.:

Synonyms:(+/-)-2-(1-(methoxycarbonyl)-5-ethyl-2-methoxycyclohexa-2,5-dienyl)acetic acid

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Chemical Property of (+/-)-2-(1-(methoxycarbonyl)-5-ethyl-2-methoxycyclohexa-2,5-dienyl)acetic acid

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Technology Process of (+/-)-2-(1-(methoxycarbonyl)-5-ethyl-2-methoxycyclohexa-2,5-dienyl)acetic acid

There total 1 articles about (+/-)-2-(1-(methoxycarbonyl)-5-ethyl-2-methoxycyclohexa-2,5-dienyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 881897-24-1
(+/-)-methyl 5-ethyl-2-methoxy-1-(tert-butoxycarbonylmethyl)cyclohexa-2,5-dienecarboxylate

: 881897-25-2
(+/-)-2-(1-(methoxycarbonyl)-5-ethyl-2-methoxycyclohexa-2,5-dienyl)acetic acid

Guidance literature:: With 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 1h;
DOI:10.1021/ol052749q

Reference yield: 69.0%

: 881897-25-2
(+/-)-2-(1-(methoxycarbonyl)-5-ethyl-2-methoxycyclohexa-2,5-dienyl)acetic acid

: N-(2-chloroallyl)hydroxylammonium trifluoroacetate

: 1-{[(2-chloro-allyl)-hydroxy-carbamoyl]-methyl}-5-ethyl-2-methoxy-cyclohexa-2,5-dienecarboxylic acid methyl ester

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; water; at 20 ℃; for 2h; pH=5;
DOI:10.1021/ol052749q

Reference yield: 69.0%

: 881897-25-2
(+/-)-2-(1-(methoxycarbonyl)-5-ethyl-2-methoxycyclohexa-2,5-dienyl)acetic acid

: N-(2-chloroallyl)-hydroxylamine

: C₁₆H₂₂ClNO₄

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; water; at 20 ℃; for 2h; pH=5;
DOI:10.1016/j.tet.2008.02.107