(2-fluoro-2-iodoethyl)benzene

Base Information

Chemical Name:(2-fluoro-2-iodoethyl)benzene
CAS No.:151588-82-8
Molecular Formula:C₈H₈FI
Molecular Weight:250.054
Hs Code.:

Synonyms:(2-fluoro-2-iodoethyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-fluoro-2-iodoethyl)benzene

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Technology Process of (2-fluoro-2-iodoethyl)benzene

There total 4 articles about (2-fluoro-2-iodoethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 457-45-4
(±)-2-fluoro-3-phenylpropanoic acid

: 151588-82-8
(2-fluoro-2-iodoethyl)benzene

Guidance literature:: With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; In 1,2-dichloro-ethane; for 6h; Reflux; Irradiation; Inert atmosphere;
DOI:10.1021/ja504089y

Reference yield:

: 1578-79-6
diethyl 2-benzyl-2-fluoromalonate

: 151588-82-8
(2-fluoro-2-iodoethyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: lithium chloride / dimethyl sulfoxide; water / Reflux; Inert atmosphere

2: lithium hydroxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

3: 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione / 1,2-dichloro-ethane / 6 h / Reflux; Irradiation; Inert atmosphere

With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; lithium chloride; lithium hydroxide; In tetrahydrofuran; water; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1021/ja504089y

Reference yield:

: 330-80-3
ethyl 2-fluoro-3-phenylpropanoate

: 151588-82-8
(2-fluoro-2-iodoethyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

2: 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione / 1,2-dichloro-ethane / 6 h / Reflux; Irradiation; Inert atmosphere

With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; lithium hydroxide; In tetrahydrofuran; water; 1,2-dichloro-ethane;
DOI:10.1021/ja504089y