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Technology Process of methylenebis

methylenebis

Base Information
  • Chemical Name:methylenebis
  • CAS No.:75375-53-0
  • Molecular Formula:C25H18As2F4
  • Molecular Weight:544.255
  • Hs Code.:
methylenebis<bis(p-fluorophenyl)arsine>

Synonyms:methylenebis

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Technology Process of methylenebis

There total 1 articles about methylenebis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methylenebis(dichloroarsine)
30077-57-7

methylenebis(dichloroarsine)

1-Bromo-4-fluorobenzene
460-00-4

1-Bromo-4-fluorobenzene

methylenebis<bis(p-fluorophenyl)arsine>
75375-53-0

methylenebis

Guidance literature:
With magnesium; Yield given. Multistep reaction; 2.) THF, boiling point, 6 h;

Reference yield: 89.7%

methylenebis<bis(p-fluorophenyl)arsine>
75375-53-0

methylenebis

C<sub>25</sub>H<sub>18</sub>As<sub>2</sub>F<sub>4</sub>S<sub>2</sub>
75375-62-1

C25H18As2F4S2

Guidance literature:
With sulfur; In toluene; for 30h; Heating;

Reference yield: 87.9%

methylenebis<bis(p-fluorophenyl)arsine>
75375-53-0

methylenebis

C<sub>25</sub>H<sub>18</sub>As<sub>2</sub>F<sub>4</sub>O<sub>2</sub>
75375-57-4

C25H18As2F4O2

Guidance literature:
With dihydrogen peroxide; In acetone; at 7 - 10 ℃; for 1h; for 3 h at room temperature;
upstream raw materials:

methylenebis(dichloroarsine)

1-Bromo-4-fluorobenzene

Downstream raw materials:

C25H18As2F4O2

C25H18As2F4S2

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