4--1-methylpiperidin-4-ol

Base Information

Chemical Name:4--1-methylpiperidin-4-ol
CAS No.:133030-42-9
Molecular Formula:C₁₄H₂₁NO₂S
Molecular Weight:267.392
Hs Code.:

4-<methoxy(phenylthio)methyl>-1-methylpiperidin-4-ol

Synonyms:4--1-methylpiperidin-4-ol

Suppliers and Price of 4--1-methylpiperidin-4-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4--1-methylpiperidin-4-ol

Chemical Property:

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Technology Process of 4--1-methylpiperidin-4-ol

There total 1 articles about 4--1-methylpiperidin-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1445-73-4
1-Methyl-4-piperidone

: 13865-50-4
methoxymethyl phenyl sulfide

: 133030-42-9
4--1-methylpiperidin-4-ol

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) hexane, THF, -30 deg C, 40 min 2.) THF, -30 deg C, 20 min;

Reference yield: 92.0%

: 133030-42-9
4--1-methylpiperidin-4-ol

: 104354-53-2
1-methyl-4-phenylthiopiperidine-4-carbaldehyde

Guidance literature:: With thionyl chloride; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 133030-42-9
4--1-methylpiperidin-4-ol

: 120749-40-8,133030-60-1
(3RS,4SR)-3,8-dimethyl-4-phenylthio-1-aza-1-oxaspiro<4.5>decane

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / CH₂Cl₂ / 0 °C

2: 1) LDA / 1) THF, -78 deg C, 2) THF, -78 deg C

3: LiAlH₄ / tetrahydrofuran / 0 °C

4: 85 percent / p-TsOH / benzene / 0.33 h / Heating

With lithium aluminium tetrahydride; thionyl chloride; toluene-4-sulfonic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; benzene;