Technology Process of C27H35FN2O6
There total 4 articles about C27H35FN2O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; iron(III) oxalate hexahydrate; Selectfluor;
In
water; acetonitrile;
at 0 ℃;
for 0.533333h;
DOI:10.1021/ja3063716
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 25 °C
2: trifluoroacetic acid / dichloromethane / 1 h
3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 25 °C
4: sodium tetrahydroborate; iron(III) oxalate hexahydrate; Selectfluor / water; acetonitrile / 0.53 h / 0 °C
With
dmap; sodium tetrahydroborate; iron(III) oxalate hexahydrate; potassium carbonate; Selectfluor; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
4: Markovnikov addition;
DOI:10.1021/ja3063716
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluoroacetic acid / dichloromethane / 1 h
2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 25 °C
3: sodium tetrahydroborate; iron(III) oxalate hexahydrate; Selectfluor / water; acetonitrile / 0.53 h / 0 °C
With
dmap; sodium tetrahydroborate; iron(III) oxalate hexahydrate; Selectfluor; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
dichloromethane; water; acetonitrile;
3: Markovnikov addition;
DOI:10.1021/ja3063716
