bis(4-chlorophenethyl)phosphine sulfide

Base Information

• Chemical Name: bis(4-chlorophenethyl)phosphine sulfide
• CAS No.: 1428677-26-2
• Molecular Formula: C₁₆H₁₇Cl₂PS
• Molecular Weight: 343.257
• Mol file: 1428677-26-2.mol

Synonyms:bis(4-chlorophenethyl)phosphine sulfide

Chemical Property of bis(4-chlorophenethyl)phosphine sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(4-chlorophenethyl)phosphine sulfide

There total 3 articles about bis(4-chlorophenethyl)phosphine sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

bis[2-(4-chlorophenyl)ethyl]phosphine (1411983-70-4) → bis(4-chlorophenethyl)phosphine sulfide (1428677-26-2)

Guidance literature:

With sulfur; In ethanol; benzene;

DOI:10.1002/ejoc.201301786

Reference yield:

4-vinylbenzyl chloride (1073-67-2,24991-47-7) → bis(4-chlorophenethyl)phosphine sulfide (1428677-26-2)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus

2: sulfur / ethanol; benzene

With phosphorus; sulfur; In ethanol; benzene;

DOI:10.1002/ejoc.201301786

Reference yield:

4-vinylbenzyl chloride (1073-67-2,24991-47-7) + phosphorus + water (7732-18-5) + potassium hydroxide → bis(4-chlorophenethyl)phosphine sulfide (1428677-26-2)

Guidance literature:

phosphorus; water; potassium hydroxide; In toluene; Inert atmosphere;

4-vinylbenzyl chloride; With dimethyl sulfoxide; potassium hydroxide; In water; Inert atmosphere;

With sulfur; Inert atmosphere;

DOI:10.1080/17415993.2015.1007143

upstream raw materials:

bis[2-(4-chlorophenyl)ethyl]phosphine

4-vinylbenzyl chloride

water

Downstream raw materials:

2-butoxyethyl[bis(4-chlorophenethyl)]phosphine sulfide

bis(4-chlorophenethyl)[2-(phenylsulfanyl)ethyl]phosphine sulfide

C₃₂H₃₂Cl₄P₂S₂Se

C₁₆H₁₇Cl₂PSSe