(Benzyl-{[(S)-1-methylcarbamoyl-2-(1-trityl-1H-imidazol-4-yl)-ethylcarbamoyl]-methyl}-amino)-acetic acid

Base Information

• Chemical Name: (Benzyl-{[(S)-1-methylcarbamoyl-2-(1-trityl-1H-imidazol-4-yl)-ethylcarbamoyl]-methyl}-amino)-acetic acid
• CAS No.: 1333228-06-0
• Molecular Formula: C₃₇H₃₇N₅O₄
• Molecular Weight: 615.732

Synonyms:(Benzyl-{[(S)-1-methylcarbamoyl-2-(1-trityl-1H-imidazol-4-yl)-ethylcarbamoyl]-methyl}-amino)-acetic acid

Chemical Property of (Benzyl-{[(S)-1-methylcarbamoyl-2-(1-trityl-1H-imidazol-4-yl)-ethylcarbamoyl]-methyl}-amino)-acetic acid

Chemical Property:

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Technology Process of (Benzyl-{[(S)-1-methylcarbamoyl-2-(1-trityl-1H-imidazol-4-yl)-ethylcarbamoyl]-methyl}-amino)-acetic acid

There total 3 articles about (Benzyl-{[(S)-1-methylcarbamoyl-2-(1-trityl-1H-imidazol-4-yl)-ethylcarbamoyl]-methyl}-amino)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nim-trityl-L-histidine N'-methylamide (145695-69-8) + N-benzyliminodiacetic anhydride acid (67305-69-5) → (Benzyl-{[(S)-1-methylcarbamoyl-2-(1-trityl-1H-imidazol-4-yl)-ethylcarbamoyl]-methyl}-amino)-acetic acid (1333228-06-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.ejmech.2014.12.005

Reference yield:

N-benzyliminodiacetic acid (3987-53-9) → (Benzyl-{[(S)-1-methylcarbamoyl-2-(1-trityl-1H-imidazol-4-yl)-ethylcarbamoyl]-methyl}-amino)-acetic acid (1333228-06-0)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic anhydride; acetic anhydride / 4 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With acetic anhydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; In N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2014.12.005

Reference yield:

N(τ)-(triphenylmethyl)-L-histidine methyl ester hydrochloride (32946-56-8) → (Benzyl-{[(S)-1-methylcarbamoyl-2-(1-trityl-1H-imidazol-4-yl)-ethylcarbamoyl]-methyl}-amino)-acetic acid (1333228-06-0)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol; ethyl [2]alcohol / Reflux

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In methanol; ethyl [2]alcohol; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2014.12.005

upstream raw materials:

N-benzyliminodiacetic acid

N(τ)-(triphenylmethyl)-L-histidine methyl ester hydrochloride

N_im-trityl-L-histidine N'-methylamide

N-benzyliminodiacetic anhydride acid

Downstream raw materials:

(benzyl-{[(S)-2-(1H-imidazol-4-yl)-1-methylcarbamoyl-ethylcarbamoyl]-methyl}-amino)-acetic acid.

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