3-[2-chloro-2-(4-chlorophenyl)ethenyl]-2，2-dimethyl cyclopropane carboxylic acid

Base Information

• Chemical Name: 3-[2-chloro-2-(4-chlorophenyl)ethenyl]-2，2-dimethyl cyclopropane carboxylic acid
• CAS No.: 73610-74-9
• Molecular Formula: C₁₄H₁₄Cl₂O₂
• Molecular Weight: 285.17

Synonyms:3-[2-chloro-2-(4-chlorophenyl)ethenyl]-2，2-dimethyl cyclopropane carboxylic acid

Chemical Property of 3-[2-chloro-2-(4-chlorophenyl)ethenyl]-2，2-dimethyl cyclopropane carboxylic acid

Chemical Property:

• Boiling Point: 424.2±40.0 °C(Predicted)
• PKA: 4.25±0.42(Predicted)
• Density: 1.366±0.06 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

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Technology Process of 3-[2-chloro-2-(4-chlorophenyl)ethenyl]-2，2-dimethyl cyclopropane carboxylic acid

There total 4 articles about 3-[2-chloro-2-(4-chlorophenyl)ethenyl]-2，2-dimethyl cyclopropane carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-acetyl-3,3-dimethyl-cyclopropane-1-carbaldehyde (77772-09-9) + 3-(2-chloro-2-(4-chlorophenyl)-vinyl)-2,2-dimethyl-cycloprop-1-yl methyl ketone + α-chloro-(4-chloro-benzyl)phosphonic acid dimethyl ester (60191-02-8) → trans-3-(2-chloro-2-(4-chloro-phenyl)-vinyl)-2,2-dimethyl-cyclopropane-1-carboxylic acid (73610-74-9)

Guidance literature:

With sodium hydroxide; bromine; sodium methylate; In tetrahydrofuran; 1,4-dioxane; hydrogenchloride; methanol; water;

Reference yield:

methanolic KOH + 4,4-dimethyl-1,3-dichloro-6-bromo-1-(4-chlorophenyl)-1-hexen-5-one → trans-3-(2-chloro-2-(4-chloro-phenyl)-vinyl)-2,2-dimethyl-cyclopropane-1-carboxylic acid (73610-74-9)

Guidance literature:

In cyclohexane;

Reference yield:

→ trans-3-(2-chloro-2-(4-chloro-phenyl)-vinyl)-2,2-dimethyl-cyclopropane-1-carboxylic acid (73610-74-9)

Guidance literature:

upstream raw materials:

2-acetyl-3,3-dimethyl-cyclopropane-1-carbaldehyde

α-chloro-(4-chloro-benzyl)phosphonic acid dimethyl ester

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