(3-{2-[2-(4-Benzyloxycarbonylamino-butyrylamino)-ethyldisulfanyl]-ethylcarbamoyl}-propyl)-carbamic acid benzyl ester

Base Information

Chemical Name:(3-{2-[2-(4-Benzyloxycarbonylamino-butyrylamino)-ethyldisulfanyl]-ethylcarbamoyl}-propyl)-carbamic acid benzyl ester
CAS No.:104071-85-4
Molecular Formula:C₂₈H₃₈N₄O₆S₂
Molecular Weight:590.765
Hs Code.:

Synonyms:(3-{2-[2-(4-Benzyloxycarbonylamino-butyrylamino)-ethyldisulfanyl]-ethylcarbamoyl}-propyl)-carbamic acid benzyl ester

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Chemical Property of (3-{2-[2-(4-Benzyloxycarbonylamino-butyrylamino)-ethyldisulfanyl]-ethylcarbamoyl}-propyl)-carbamic acid benzyl ester

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of (3-{2-[2-(4-Benzyloxycarbonylamino-butyrylamino)-ethyldisulfanyl]-ethylcarbamoyl}-propyl)-carbamic acid benzyl ester

There total 3 articles about (3-{2-[2-(4-Benzyloxycarbonylamino-butyrylamino)-ethyldisulfanyl]-ethylcarbamoyl}-propyl)-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 104071-83-2
[3-(2-Mercapto-ethylcarbamoyl)-propyl]-carbamic acid benzyl ester

: 104071-85-4
(3-{2-[2-(4-Benzyloxycarbonylamino-butyrylamino)-ethyldisulfanyl]-ethylcarbamoyl}-propyl)-carbamic acid benzyl ester

Guidance literature:: With iodine; In water; acetic acid; for 0.25h; Ambient temperature;
DOI:10.1021/jm00161a015

Reference yield:

: 5105-78-2
4-(benzyloxycarbonylamino)butyric acid

: 104071-85-4
(3-{2-[2-(4-Benzyloxycarbonylamino-butyrylamino)-ethyldisulfanyl]-ethylcarbamoyl}-propyl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 33 percent / phosphonitrilic chloride (t-PNC), Et₃N / tetrahydrofuran / 0 - 20 °C

2: 60 percent / MeONa/MeOH / 1 h / Ambient temperature

3: 66 percent / I₂ / acetic acid; H₂O / 0.25 h / Ambient temperature

With methanol; 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; iodine; sodium methylate; triethylamine; In tetrahydrofuran; water; acetic acid;
DOI:10.1021/jm00161a015

Reference yield:

: 97314-02-8
Thioacetic acid S-[2-(4-benzyloxycarbonylamino-butyrylamino)-ethyl] ester

: 104071-85-4
(3-{2-[2-(4-Benzyloxycarbonylamino-butyrylamino)-ethyldisulfanyl]-ethylcarbamoyl}-propyl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / MeONa/MeOH / 1 h / Ambient temperature

2: 66 percent / I₂ / acetic acid; H₂O / 0.25 h / Ambient temperature

With methanol; iodine; sodium methylate; In water; acetic acid;
DOI:10.1021/jm00161a015