(1'RS,2'SR)-1-<3'-(t-butyldiphenylsiloxy)-2'-methyl-1'-(phenylthio)propyl>cyclopentene

Base Information

Chemical Name:(1'RS,2'SR)-1-<3'-(t-butyldiphenylsiloxy)-2'-methyl-1'-(phenylthio)propyl>cyclopentene
CAS No.:133030-68-9
Molecular Formula:C₃₁H₃₈OSSi
Molecular Weight:486.794
Hs Code.:

Synonyms:(1'RS,2'SR)-1-<3'-(t-butyldiphenylsiloxy)-2'-methyl-1'-(phenylthio)propyl>cyclopentene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1'RS,2'SR)-1-<3'-(t-butyldiphenylsiloxy)-2'-methyl-1'-(phenylthio)propyl>cyclopentene

Chemical Property:

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Technology Process of (1'RS,2'SR)-1-<3'-(t-butyldiphenylsiloxy)-2'-methyl-1'-(phenylthio)propyl>cyclopentene

There total 4 articles about (1'RS,2'SR)-1-<3'-(t-butyldiphenylsiloxy)-2'-methyl-1'-(phenylthio)propyl>cyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 133030-63-4
(1RS,2RS)-3-(t-butyldiphenylsiloxy)-2-methyl-1-<1-(phenylthio)cyclopentyl>propan-1-ol

: 133030-68-9
(1'RS,2'SR)-1-<3'-(t-butyldiphenylsiloxy)-2'-methyl-1'-(phenylthio)propyl>cyclopentene

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 0.0666667h; Heating;

Reference yield:

: 115205-40-8
1-phenylsulfanylcyclopentane carboxaldehyde

: 133030-68-9
(1'RS,2'SR)-1-<3'-(t-butyldiphenylsiloxy)-2'-methyl-1'-(phenylthio)propyl>cyclopentene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) LDA / 1.) THF, -78 degC, 10 min 2.) -78 degC, 5 min

2: 85 percent / LiAlH₄ / diethyl ether / 4 h / 0 °C

3: 83 percent / imidazole / dimethylformamide / 24 h / Ambient temperature

4: 100 percent / TsOH / benzene / 0.07 h / Heating

With 1H-imidazole; lithium aluminium tetrahydride; toluene-4-sulfonic acid; lithium diisopropyl amide; In diethyl ether; N,N-dimethyl-formamide; benzene;

Reference yield:

: 120749-37-3,133030-55-4,138751-07-2
(1RS,2RS)-2-methyl-1-<1-(phenylthio)cyclopentyl>propane-1,3-diol

: 133030-68-9
(1'RS,2'SR)-1-<3'-(t-butyldiphenylsiloxy)-2'-methyl-1'-(phenylthio)propyl>cyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / imidazole / dimethylformamide / 24 h / Ambient temperature

2: 100 percent / TsOH / benzene / 0.07 h / Heating

With 1H-imidazole; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; benzene;