Technology Process of (E)-6-cyclohexylidene-3-methylhex-2-en-1-ol
There total 11 articles about (E)-6-cyclohexylidene-3-methylhex-2-en-1-ol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C19H26O3S;
With
lithium triethylborohydride;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Inert atmosphere;
With
(1,2-bis(diphenylphosphino)ethane)palladium(II) chloride;
In
tetrahydrofuran;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1002/adsc.201100215
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C
1.2: -40 - 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
3.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere
4.1: sodium ethanolate / ethanol / 0 °C
4.2: 16 h / 0 - 20 °C
5.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C
6.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C
6.2: -40 - 20 °C
7.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
With
lithium aluminium tetrahydride; 15-crown-5; sodium ethanolate; phosphorus tribromide; sodium hydride; potassium hydroxide;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; water; mineral oil;
